6-P-TOLYLPYRIDIN-3-YLAMINE
- Product Name
- 6-P-TOLYLPYRIDIN-3-YLAMINE
- CAS No.
- 170850-45-0
- Chemical Name
- 6-P-TOLYLPYRIDIN-3-YLAMINE
- Synonyms
- 6-(p-Tolyl);AKOS BAR-2341;6-(p-tolyl)pyridin-3-aMine;6-P-TOLYLPYRIDIN-3-YLAMINE;3-AMINO-6-(4-TOLYL)PYRIDINE;6-P-TOLYLPYRIDIN-3-YLAMINE, 95+%;6-(4-methylphenyl)pyridin-3-amine;3-Pyridinamine, 6-(4-methylphenyl)-
- CBNumber
- CB4354215
- Molecular Formula
- C12H12N2
- Formula Weight
- 184.24
- MOL File
- 170850-45-0.mol
6-P-TOLYLPYRIDIN-3-YLAMINE Property
- Boiling point:
- 351.1±27.0 °C(Predicted)
- Density
- 1.106±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 5.68±0.25(Predicted)
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- P769083
- Product name
- 6-(p-tolyl)pyridin-3-amine
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- Z4276
- Product name
- 6-(p-Tolyl)pyridin-3-amine
- Packaging
- 250mg
- Price
- $119
- Updated
- 2021/12/16
- Product number
- OR913128
- Product name
- 6-P-Tolylpyridin-3-ylamine
- Purity
- 98%
- Packaging
- 1g
- Price
- $130
- Updated
- 2021/12/16
- Product number
- 3H30-1-QJ
- Product name
- 6-p-Tolylpyridin-3-ylamine
- Purity
- 98%
- Packaging
- 1g
- Price
- $208
- Updated
- 2021/12/16
- Product number
- COR0003670
- Product name
- 6-P-TOLYLPYRIDIN-3-YLAMINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $228.9
- Updated
- 2021/12/16
6-P-TOLYLPYRIDIN-3-YLAMINE Chemical Properties,Usage,Production
Synthesis
131941-26-9
170850-45-0
4.3.1 Synthesis of 4'-methyl-4-aminobiphenyl (4a): 5-nitro-2-(p-tolyl)pyridine (3a, 2.54 mmol, 541 mg) was dissolved in a solvent mixture of EtOH/EtOAc (1:1, 50 mL). The hydrogenation-reduction reaction was carried out in all-hydrogen mode in the presence of Raney Nickel catalyst at a reaction temperature of 65 °C and a hydrogen flow rate of 0.8 mL/min. Upon completion of the reaction, the resulting solution was concentrated under reduced pressure to give 480 mg of yellow solid. The crude product was purified by silica gel column chromatography using hexane/CH2Cl2 (1:1) as eluent, resulting in 440 mg of the pure target product 4'-methyl-4-aminobiphenyl (4a) as an off-white solid in 95% yield.
References
[1] Tetrahedron, 2012, vol. 68, # 45, p. 9272 - 9277
6-P-TOLYLPYRIDIN-3-YLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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