5-CHLORO-4-METHYL-2-NITROANILINE
- Product Name
- 5-CHLORO-4-METHYL-2-NITROANILINE
- CAS No.
- 7149-80-6
- Chemical Name
- 5-CHLORO-4-METHYL-2-NITROANILINE
- Synonyms
- SKL336;NSC 72334;-2-nitroaniL;TIMTEC-BB SBB003703;5-CHLORO-2-NITRO-P-TOLUIDINE;4-Amino-2-chloro-5-nitrotoluene;5-CHLORO-4-METHYL-2-NITROANILINE;5-Chloro-4-methyl-2-nitroaniline,96%;5-Chloro-4-methyl-2-nitroaniline, 95+%;Benzenamine, 5-chloro-4-methyl-2-nitro-
- CBNumber
- CB4354907
- Molecular Formula
- C7H7ClN2O2
- Formula Weight
- 186.6
- MOL File
- 7149-80-6.mol
5-CHLORO-4-METHYL-2-NITROANILINE Property
- Melting point:
- 159-163 °C
- Boiling point:
- 339.3±37.0 °C(Predicted)
- Density
- 1.415±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Crystalline Powder
- pka
- -0.79±0.25(Predicted)
- color
- Orange-brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C349870
- Product name
- 5-Chloro-4-methyl-2-nitroaniline
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- C349870
- Product name
- 5-Chloro-4-methyl-2-nitroaniline
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- CS-W016875
- Product name
- 5-Chloro-4-methyl-2-nitroaniline
- Purity
- 99.66%
- Packaging
- 5g
- Price
- $47
- Updated
- 2021/12/16
- Product number
- 076174
- Product name
- 5-Chloro-4-methyl-2-nitroaniline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $59
- Updated
- 2021/12/16
- Product number
- FC139748
- Product name
- 5-Chloro-4-methyl-2-nitroaniline
- Packaging
- 5G
- Price
- $63
- Updated
- 2021/12/16
5-CHLORO-4-METHYL-2-NITROANILINE Chemical Properties,Usage,Production
Chemical Properties
orange-brown crystalline powder
Synthesis
7149-78-2
7149-80-6
(b) Preparation of the intermediate compound 5-chloro-4-methyl-2-nitroaniline: Sodium ethoxide (8.27 g, 45.9 mmol) was dissolved in ethanol (10 mL) to prepare a sodium ethoxide solution. The solution was slowly added to a solution of ethanol (10 mL) containing N-(2-nitro-4-methyl-5-chlorophenyl)acetamide (7.0 g, 30.6 mmol) with stirring at room temperature. After 1 hour of reaction, the reaction mixture was poured into water (100 mL) and precipitate was precipitated. The precipitate was collected by filtration and washed with a mixture of isopropanol and n-hexane (1:3, 10 mL) followed by n-hexane (10 mL) to give 5.71 g (85% yield) of 5-chloro-4-methyl-2-nitroaniline. Mass spectrometry (MS) showed a m/z of 187.0 (M + 1).
References
[1] Patent: WO2010/19208, 2010, A1. Location in patent: Page/Page column 167-168
[2] Journal of Medicinal Chemistry, 1992, vol. 35, # 23, p. 4455 - 4463
[3] Journal of Heterocyclic Chemistry, 1981, vol. 18, p. 1635 - 1636
[4] Patent: WO2011/23812, 2011, A1. Location in patent: Page/Page column 164
5-CHLORO-4-METHYL-2-NITROANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-CHLORO-4-METHYL-2-NITROANILINE manufacturers
- Product
- 5-CHLORO-4-METHYL-2-NITROANILINE 7149-80-6
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-09