ChemicalBook > CAS DataBase List > 5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE

5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE

Product Name
5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE
CAS No.
53525-65-8
Chemical Name
5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE
Synonyms
SPECS AN-584/43226970;Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione;Diimidazo[1,5-a:1’,5’-d)pyrazine-5,10-dione,HCl;5H,10H-diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione;Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione, DiHCl;5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE;5H,10H-DiiMidazo[1,5-a:1', 5'-d] pyrazine-5,10-dione b;5H,10H-Diimidazo[1,5-A:1', 5'-D] pyrazine-5,10-dione ,98%;Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione, dihydrochloride
CBNumber
CB4438599
Molecular Formula
C8H4N4O2
Formula Weight
188.14
MOL File
53525-65-8.mol
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5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE Property

storage temp. 
2-8°C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P330Rinse mouth.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
D680050
Product name
5H,10H-Diimidazo[1,5-A:1'',5''-D]pyrazine-5,10-dione
Packaging
10mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
V6475
Product name
Diimidazo[1,5-a:1'',5''-d]pyrazine-5,10-dioneDiHCl
Packaging
5g
Price
$1230
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0029240
Product name
DIIMIDAZO[1,5-A:1',5'-D]PYRAZINE-5,10-DIONE
Purity
95.00%
Packaging
1KG
Price
$11896.5
Updated
2021/12/16
Ambeed
Product number
A159530
Product name
Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione
Purity
95%
Packaging
100mg
Price
$42
Updated
2021/12/16
Crysdot
Product number
CD11109219
Product name
Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione
Purity
95+%
Packaging
25g
Price
$1980
Updated
2021/12/16
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5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE Chemical Properties,Usage,Production

Synthesis

1072-84-0

53525-65-8

General procedure for the synthesis of imidazo[1,5-a:1',5'-d]pyrazine-5,10-dione from 1H-imidazole-4-carboxylic acid: 1H-imidazole-4-carboxylic acid (5 g, 44.6 mmol) was suspended in thionyl chloride (75 mL), and heated and refluxed under stirring for 18 hours. After completion of the reaction, the reaction mixture was cooled, filtered, washed with toluene and dried under high vacuum to afford the target compound imidazo[1,5-a:1',5'-d]pyrazine-5,10-dione as a yellow solid in 95% yield. Molecular formula: C8H4N4O2, molecular weight: 188.14 g/mol, melting point: 265-268°C. 1H NMR (300 MHz, DMSO-d6) δ: 8.24 (d, 1H, CHC-CO), 8.32 (d, 1H, CHC-CO, J=3Hz), 8.88 (d, 1H, CHN), 9.28 (d, 1H , CHN, J=3Hz).13C NMR (100 MHz, DMSO-d6) δ: 123.99, 124.52, 125.62, 137.26, 139.73, 150.39, 159.68.MS (ESI+, QTof, m/z): 189.0 [M + H]+.

References

[1] Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 13, p. 6601 - 6610
[2] European Journal of Medicinal Chemistry, 2017, vol. 138, p. 909 - 919
[3] Pharmaceutical Chemistry Journal, 1986, vol. 20, # 7, p. 460 - 463
[4] Khimiko-Farmatsevticheskii Zhurnal, 1986, vol. 20, # 7, p. 799 - 802
[5] Patent: EP1439169, 2004, A1. Location in patent: Page 81-82

5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE Preparation Products And Raw materials

Raw materials

Preparation Products

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5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE Suppliers

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53525-65-8, 5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONERelated Search:


  • SPECS AN-584/43226970
  • 5H,10H-DIIMIDAZO[1,5-A:1', 5'-D] PYRAZINE-5,10-DIONE
  • Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione, dihydrochloride
  • Diimidazo[1,5-a:1’,5’-d)pyrazine-5,10-dione,HCl
  • 5H,10H-Diimidazo[1,5-A:1', 5'-D] pyrazine-5,10-dione ,98%
  • 5H,10H-DiiMidazo[1,5-a:1', 5'-d] pyrazine-5,10-dione b
  • Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione, DiHCl
  • Diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione
  • 5H,10H-diimidazo[1,5-a:1',5'-d]pyrazine-5,10-dione
  • 53525-65-8
  • C8H4N4O2
  • C8H6Cl2N4O2
  • blocks
  • BuildingBlocks
  • Imidazoles
  • Pyridines