FDA Approval
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Dotinurad

FDA Approval
Product Name
Dotinurad
CAS No.
1285572-51-1
Chemical Name
Dotinurad
Synonyms
Dotinurad;Duotenuode;Duotenuolei;Doltenolil control;Dotinurad (FYU-981);Dotinurad, 10 mM in DMSO;3-(3,5-dichloro-4-hydroxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole;(3,5-Dichloro-4-hydroxyphenyl)(1,1-dioxido-3(2H)-benzothiazolyl)methanone;(3,5-dichloro-4-hydroxyphenyl)(1,1-dioxidobenzo[d]thiazol-3(2H)-yl)methanone;Methanone, (3,5-dichloro-4-hydroxyphenyl)(1,1-dioxido-3(2H)-benzothiazolyl)-
CBNumber
CB44667832
Molecular Formula
C14H9Cl2NO4S
Formula Weight
358.2
MOL File
1285572-51-1.mol
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Dotinurad Property

Melting point:
188 - 191°C
Boiling point:
614.8±55.0 °C(Predicted)
Density 
1.662±0.06 g/cm3(Predicted)
storage temp. 
-20°C Freezer, Under inert atmosphere
solubility 
Chloroform (Slightly, Sonicated), DMSO (Sparingly)
pka
4.60±0.25(Predicted)
form 
Solid
color 
White to Off-White
InChI
InChI=1S/C14H9Cl2NO4S/c15-9-5-8(6-10(16)13(9)18)14(19)17-7-22(20,21)12-4-2-1-3-11(12)17/h1-6,18H,7H2
InChIKey
VOFLAIHEELWYGO-UHFFFAOYSA-N
SMILES
C(C1=CC(Cl)=C(O)C(Cl)=C1)(N1C2=CC=CC=C2S(=O)(=O)C1)=O
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

ChemScene
Product number
CS-0030545
Product name
Dotinurad
Purity
98.10%
Packaging
5mg
Price
$350
Updated
2021/12/16
ChemScene
Product number
CS-0030545
Product name
Dotinurad
Purity
98.10%
Packaging
10mg
Price
$550
Updated
2021/12/16
ChemScene
Product number
CS-0030545
Product name
Dotinurad
Purity
98.10%
Packaging
25mg
Price
$990
Updated
2021/12/16
ChemScene
Product number
CS-0030545
Product name
Dotinurad
Purity
98.10%
Packaging
50mg
Price
$1650
Updated
2021/12/16
ChemScene
Product number
CS-0030545
Product name
Dotinurad
Purity
98.10%
Packaging
100mg
Price
$2250
Updated
2021/12/16
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Dotinurad Chemical Properties,Usage,Production

FDA Approval

Dotinurad was approved by the FDA in 2015.

Description

Dotinurad is an organic compound with the chemical Name (3,5-dichloro-4-hydroxyphenyl)(1,1-dioxidobenzo[d]thiazol-3(2H)-yl)methanone. This compound is a newer urate-lowering agent that suppresses uric acid reabsorption through the selective inhibition of urate transporter 1 (URAT1) in the proximal renal tubules, and it was first approved in Japan in 2020 for the treatment of hyperuricemia, irrespective of gout[1].

Uses

Dotinurad is a useful drug for treating hyperuricemia and gout.

brand name

URECE

Pharmacokinetics

The plasma concentration of dotinurad increased in a dose-dependent manner with Cmax and AUC0–24h values of 107 μg/ml and 780 μg.h/ml, respectively, at a dose of 30 mg/kg. Dotinurad dose-dependently lowered the plasma urate levels with its maximum effect at 8 h. Changes in plasma urate level between 0 and 8 h (ΔPUA) were lower than that of control by 0.28, 0.97 (p < 0.05), and 1.79 mg/dl (p < 0.01), at doses of 1, 5, and 30 mg/kg, respectively. Furthermore, dotinurad dose-dependently increased FEUA. The 0–4 h FEUA increased by 180%, at a dose of 30 mg/kg compared to the control (p < 0.01)[3].    

Synthesis

Aminothiophenol (152) reacts with hydrated formaldehyde to give dihydrobenzothiazole 153. Acid chloride 155 is generated from acid 154. Dihydrobenzothiazole 153 is condensed with acid chloride 155 to form amide 156. Thiazole is oxidized using mCPBA. Methyl ether is removed in the presence of lithium chloride to give doxenolide.

Advantages

Dotinurad, as a selective urate reabsorption inhibitor, is anticipated to be more effective in inhibiting urate reabsorption compared to conventional urate-lowering agents. It demonstrates noninferiority to benzbromarone or febuxostat in reducing serum urate levels in hyperuricemic patients with or without gout. Moreover, its effectiveness remains uncompromised in patients with mild to moderate renal or hepatic impairment. In a long-term study, a majority of patients achieved the target serum urate level of ≤6 mg/dL when administered a maintenance dose of 2 or 4 mg once daily. No safety concerns, such as liver injury, were observed. Consequently, Dotinurad is expected to serve as a new therapeutic option for hyperuricemic patients, regardless of the presence of gout [2].

References

[1] Tanaka A, et al. Clinical effects of a selective urate reabsorption inhibitor dotinurad in patients with hyperuricemia and treated hypertension: a multicenter, prospective, exploratory study (DIANA). European Journal of Medical Research, 2023; 238.
[2] Ishikawa T, et al. Dotinurad: a novel selective urate reabsorption inhibitor for the treatment of hyperuricemia and gout. Expert Opinion on Pharmacotherapy, 2021; 22: 1397-1406.
[3] Taniguchi T, et al. Pharmacological Evaluation of Dotinurad, a Selective Urate Reabsorption Inhibitor. Journal of Pharmacology and Experimental Therapeutics, 2019; 162-170.

Dotinurad Preparation Products And Raw materials

Raw materials

Preparation Products

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Dotinurad Suppliers

SICHUAN TIANDAO PHARMACEUTICAL CO.,LTD
Tel
028-13350092412 13350092412
Email
pany01@creditpharma.com
Country
China
ProdList
10
Advantage
58
NANJING TOMMLAB PHARMATECH Co.,LTD
Tel
--
Fax
--
Email
litianang@caremo.com.cn
Country
China
ProdList
483
Advantage
58
Wuhan HSN Pharmaresearch CO., LTD.
Tel
027-81525288 18086100502
Fax
027-86589137
Email
linwell@126.com
Country
China
ProdList
233
Advantage
50
Jinan Guoding Pharmaceutical Technology Co., Ltd.
Tel
053167801621 15665775653
Fax
053167801621
Email
sales@guodingpharma.com
Country
China
ProdList
491
Advantage
58
Shanghai Wishpharma Co.,Ltd.
Tel
021-56789108 18694901298
Fax
021-56789108
Email
95413064@qq.com
Country
China
ProdList
299
Advantage
56
Huadong Microbiology Co., Ltd.
Tel
15858880160
Email
dingya@eastchinapharm.com
Country
China
ProdList
88
Advantage
58
Hubei widely chemical technology Co., Ltd.
Tel
027-59402396 13419635609
Fax
027-83989310
Email
13419635609@163.com
Country
China
ProdList
1987
Advantage
55
NANJING WEDO PHARMATECH CO.,LTD.
Tel
15189836218
Email
wedo-chem@huawe.com
Country
China
ProdList
275
Advantage
58
Chengdu Sino-Strong Pharmaceutical Co.,Ltd.
Tel
0086-28-68252565 13808081195
Fax
028-82783880
Email
2668085633@qq.com
Country
China
ProdList
212
Advantage
60
NanJing Vtrying Pharmatech Co.,Ltd
Tel
17314186806
Email
Vtrying_sale@163.com
Country
China
ProdList
140
Advantage
58
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View Lastest Price from Dotinurad manufacturers

Shanghai Wish Pharma Co., Ltd
Product
Dotinurad 1285572-51-1
Price
US $0.00-0.00/g
Min. Order
50g
Purity
Minimum 99%
Supply Ability
50kg
Release date
2025-11-06
Shaanxi Dideu New Materials Co. Ltd
Product
Dotinurad 1285572-51-1
Price
US $0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1000kg
Release date
2025-06-12
Guangzhou Tosun Pharmaceutical Ltd
Product
Dotinurad 1285572-51-1
Price
US $0.00-0.00/kg
Min. Order
5kg
Purity
98%-102%
Supply Ability
200kg
Release date
2024-12-27

1285572-51-1, DotinuradRelated Search:


  • Dotinurad
  • Methanone, (3,5-dichloro-4-hydroxyphenyl)(1,1-dioxido-3(2H)-benzothiazolyl)-
  • Dotinurad (FYU-981)
  • (3,5-dichloro-4-hydroxyphenyl)(1,1-dioxidobenzo[d]thiazol-3(2H)-yl)methanone
  • uricosuric,Inhibitor,Dotinurad,URAT1,urate,reabsorption,SLC22A12,Urate transporter 1,inhibit,transporter
  • (3,5-Dichloro-4-hydroxyphenyl)(1,1-dioxido-3(2H)-benzothiazolyl)methanone
  • 3-(3,5-dichloro-4-hydroxybenzoyl)-1,1-dioxo-2,3-dihydro-1,3-benzothiazole
  • Dotinurad, 10 mM in DMSO
  • Doltenolil control
  • Duotenuolei
  • Duotenuode
  • 1285572-51-1
  • API