N-(CINNAMOYL)-3-METHOXYANILINE

Product Name: N-(CINNAMOYL)-3-METHOXYANILINE
CAS No.: 127033-74-3
Chemical Name: N-(CINNAMOYL)-3-METHOXYANILINE
Synonyms: N-(3-methoxyphenyl)cinnamamide;SKL779;FMX14267-B1;3-methoxy-cinnamanilide;Brexpiprazole Impurity 200;N-(CINNAMOYL)-3-METHOXYANILINE;(E)-N-(3-methoxyphenyl)-3-phenylprop-2-enamide;(E)-N-(3-Methoxyphenyl)-3-phenyl-2-propenaMide;(2E)-N-(3-Methoxyphenyl)-3-phenyl-2-propenamide;(2E)-N-(3-methoxyphenyl)-3-phenylprop-2-enamide
CBNumber: CB4648626
Molecular Formula: C16H15NO2
Formula Weight: 253.3
MOL File: Mol file

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N-(CINNAMOYL)-3-METHOXYANILINE Property

Melting point:: 118-120°C
Boiling point:: 463.0±45.0 °C(Predicted)
Density: 1.176±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
solubility: DMSO
form: Solid
pka: 13.52±0.70(Predicted)
color: Off-White

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C442060
Product name: N-(Cinnamoyl)-3-methoxyaniline
Packaging: 250mg
Price: $360
Updated: 2021/12/16

AK Scientific

Product number: 7001CD
Product name: N-(Cinnamoyl)-3-methoxyaniline
Packaging: 5g
Price: $108
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC20449
Product name: N-(Cinnamoyl)-3-methoxyaniline
Packaging: 50mg
Price: $140
Updated: 2021/12/16

AK Scientific

Product number: 7001CD
Product name: N-(Cinnamoyl)-3-methoxyaniline
Packaging: 10g
Price: $142
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC20449
Product name: N-(Cinnamoyl)-3-methoxyaniline
Packaging: 100mg
Price: $255
Updated: 2021/12/16

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N-(CINNAMOYL)-3-METHOXYANILINE Chemical Properties,Usage,Production

Chemical Properties

Off-White Solid

Uses

N-(Cinnamoyl)-3-methoxyaniline (cas# 127033-74-3) is a compound useful in organic synthesis.

Synthesis

536-90-3

102-92-1

127033-74-3

To a solvent mixture of acetone (8 mL) and water (16 mL), m-aminoanisole (1 g, 8.12 mmol), potassium carbonate (1.68 g, 12.18 mmol), and 3-phenyl-2-propenoyl chloride (1.62 g, 9.74 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 30 minutes. After completion of the reaction, the mixture was poured into ice water and extracted with ethyl acetate (EtOAc). The organic phases were combined and concentrated under reduced pressure to afford N-(3-methoxyphenyl)cinnamamide (compound 3) in 98% yield.

References

[1] Patent: CN108101926, 2018, A. Location in patent: Paragraph 0030; 0031; 0032
[2] Tetrahedron Letters, 1999, vol. 40, # 24, p. 4505 - 4506
[3] Patent: CN107098855, 2017, A. Location in patent: Paragraph 0036; 0037
[4] Zhurnal Obshchei Khimii, 1940, vol. 10, p. 43,50
[5] Chem. Zentralbl., 1940, vol. 111, # II, p. 202

N-(CINNAMOYL)-3-METHOXYANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(CINNAMOYL)-3-METHOXYANILINE Suppliers

Canada 1 China 51 Germany 1 India 2 United Kingdom 1 United States 4 Global 60

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View Lastest Price from N-(CINNAMOYL)-3-METHOXYANILINE manufacturers

Career Henan Chemical Co

Product: N-(CINNAMOYL)-3-METHOXYANILINE 127033-74-3
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-100kg
Release date: 2020-01-10

127033-74-3, N-(CINNAMOYL)-3-METHOXYANILINERelated Search:

N-(CINNAMOYL)-3-METHOXYANILINE

(E)-N-(3-Methoxyphenyl)-3-phenyl-2-propenaMide

3-methoxy-cinnamanilide

(2E)-N-(3-Methoxyphenyl)-3-phenyl-2-propenamide

FMX14267-B1

N-(3-methoxyphenyl)cinnamamide

(2E)-N-(3-methoxyphenyl)-3-phenylprop-2-enamide

2-Propenamide, N-(3-methoxyphenyl)-3-phenyl-, (2E)-

(E)-N-(3-methoxyphenyl)-3-phenylprop-2-enamide

SKL779

Brexpiprazole Impurity 200

127033-74-3

Aromatics, Pharmaceuticals, Intermediates & Fine Chemicals

Aromatics Compounds

Aromatics

Intermediates & Fine Chemicals

Pharmaceuticals