4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID

Product Name: 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID
CAS No.: 914636-20-7
Chemical Name: 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID
Synonyms: 5-Carboxy-2-iodobenzotrifluoride;4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID;4-Iodo-3-(trifluoromethyl)benzoicacid99%;Benzoic acid, 4-iodo-3-(trifluoromethyl)-;4-Iodo-3-(trifluoromethyl)benzoic acid 99%
CBNumber: CB4654010
Molecular Formula: C8H4F3IO2
Formula Weight: 316.02
MOL File: Mol file

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4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Property

Boiling point:: 311.7±42.0 °C(Predicted)
Density: 2.005±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 3.59±0.10(Predicted)
form: crystalline needles
color: Tan/brown
Sensitive: Light Sensitive/Air Sensitive

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Safety

Hazard Codes: Xi
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC9306
Product name: 4-Iodo-3-(trifluoromethyl)benzoicacid
Purity: 98%
Packaging: 5g
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 1g
Price: $104
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 5G
Price: $384
Updated: 2021/12/16

AK Scientific

Product number: 7983DC
Product name: 4-Iodo-3-(trifluoromethyl)benzoicacid
Packaging: 5g
Price: $465
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 10g
Price: $688
Updated: 2021/12/16

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4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

400-76-0

914636-20-7

General procedure for the synthesis of 4-iodo-3-(trifluoromethyl)benzoic acid from 3-trifluoromethyl-4-aminobenzoic acid: 4-amino-3-trifluoromethylbenzoic acid (1.8 g, 8.8 mmol) was suspended in 30 mL of hydrochloric acid. An aqueous solution (15 mL) of sodium nitrite (0.76 g, 11.0 mmol) was slowly added dropwise at 0°C. The reaction mixture was stirred at 0-10 °C for 30 min. Subsequently, an aqueous solution (25 mL) of potassium iodide (14.6 g, 88 mmol) was added dropwise. The mixture was stirred at room temperature for 1 hour. After completion of the reaction, the product was extracted with ethyl acetate (80 mL) and the organic layer was washed with brine (80 mL). The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by fast chromatography using a gradient elution with ethyl acetate/hexane, resulting in 4-iodo-3-(trifluoromethyl)benzoic acid (2.4 g, 86% yield) as a solid.LC-ES/MS analysis showed m/e 339.3 (M+23) and 315.0 (M-1).

References

[1] Patent: WO2007/140174, 2007, A2. Location in patent: Page/Page column 42

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Suppliers

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914636-20-7, 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACIDRelated Search:

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID

4-Iodo-3-(trifluoromethyl)benzoic acid 99%

5-Carboxy-2-iodobenzotrifluoride

4-Iodo-3-(trifluoromethyl)benzoicacid99%

Benzoic acid, 4-iodo-3-(trifluoromethyl)-

914636-20-7