(IODOMETHYL)CYCLOHEXANE

Product Name: (IODOMETHYL)CYCLOHEXANE
CAS No.: 5469-33-0
Chemical Name: (IODOMETHYL)CYCLOHEXANE
Synonyms: CYCLOHEXYLIODOMETHANE;(IODOMETHYL)CYCLOHEXANE;Cyclohexane, (iodoMethyl)-;Benzo[b]thiophene-2-carboxylicacid,5,8-dimethoxy-,methylester
CBNumber: CB4679697
Molecular Formula: C7H13I
Formula Weight: 224.08
MOL File: 5469-33-0.mol

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(IODOMETHYL)CYCLOHEXANE Property

Melting point:: 175-178 °C
Boiling point:: 86.5-87.5 °C(Press: 20-21 Torr)
Density: 1.542 g/cm3(Temp: 14.2 °C)
storage temp.: 2-8°C(protect from light)
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I737695
Product name: (Iodomethyl)cyclohexane
Packaging: 500mg
Price: $310
Updated: 2021/12/16

AK Scientific

Product number: 4784AJ
Product name: (Iodomethyl)cyclohexane
Packaging: 250mg
Price: $120
Updated: 2021/12/16

AK Scientific

Product number: 4784AJ
Product name: (Iodomethyl)cyclohexane
Packaging: 5g
Price: $817
Updated: 2021/12/16

AK Scientific

Product number: 4784AJ
Product name: (Iodomethyl)cyclohexane
Packaging: 1g
Price: $224
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0009316
Product name: (IODOMETHYL)CYCLOHEXANE
Purity: 95.00%
Packaging: 1KG
Price: $6955.13
Updated: 2021/12/16

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(IODOMETHYL)CYCLOHEXANE Chemical Properties,Usage,Production

Synthesis

100-49-2

5469-33-0

Under nitrogen protection, cyclohexanemethanol (5.00 mL, 40.7 mmol) was dissolved in dichloromethane (101 mL) and cooled to 0 °C. Imidazole (3.6 g, 52.9 mmol), triphenylphosphine (13.9 g, 52.9 mmol) and iodine (13.4 g, 52.9 mmol) were added sequentially and the reaction mixture was stirred for 30 minutes. After completion of the reaction, dichloromethane was added to the reaction solution. The organic layer was washed sequentially with water and aqueous sodium thiosulfate, and the organic layer was dried with anhydrous sodium sulfate and subsequently concentrated. The concentrate was filtered through diatomaceous earth to further concentrate the filtrate. Finally, the crude product obtained was purified by silica gel column chromatography (80 g of silica gel, pentane as eluent) to give the colorless oily product (iodomethyl)cyclohexane (5.82 g, 64% yield).

References

[1] Patent: JP2017/119691, 2017, A. Location in patent: Paragraph 0179
[2] Chemische Berichte, 1907, vol. 40, p. 4865
[3] Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1906, vol. 142, p. 344
[4] Bulletin de la Societe Chimique de France, 1906, vol. <3> 35, p. 548
[5] Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1906, vol. 142, p. 344

(IODOMETHYL)CYCLOHEXANE Preparation Products And Raw materials

Raw materials

Preparation Products

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(IODOMETHYL)CYCLOHEXANE Suppliers

China 59 Germany 1 India 1 United States 7 Global 68

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View Lastest Price from (IODOMETHYL)CYCLOHEXANE manufacturers

Shanghai Yongzeng Technology Co.,Ltd

Product: (Iodomethyl)cyclohexane 5469-33-0
Price: US $0.00/gm
Min. Order: 10gm
Purity: 97%min
Supply Ability: 1kgs
Release date: 2024-09-11

5469-33-0, (IODOMETHYL)CYCLOHEXANERelated Search:

19-IODO-5-ANDROSTENE-3BETA-OL-17-ONE 3-ACETATE SPECS AB-131/42302922 DECAHYDRO-2-(IODOMETHYL)-NAPHTHALENE (IODOMETHYL)CYCLOHEXANE 19-IODO-5-CHOLESTEN-3BETA-OL 3-ACETATE 19-IODOCHOLESTEROL AKOS BBS-00002001 10-(IODOMETHYL)-13-METHYL-2,3,6,7,8,9,10,11,12,13,14,15,16,17-TETRADECAHYDRO-1H-CYCLOPENTA[A]PHENANTHRENE-3,17-DIONE 1,3,5(10)-ESTRATRIEN-17ALPHA-IODO-3,17BETA-DIOL 5,16-ANDROSTADIEN-17-IODO-3-BETA-OL AKOS BBS-00002000 2-(Iodomethyl)norcamphane BOC-AMINOCYCLOHEXANE-4-IODOMETHYL AKOS BBS-00002001 TRANS-1-BOC-AMINOMETHYL-4-IODOMETHYL-CYCLOHEXANE METHYL 4-IODOCUBANECARBOXYLATE

CYCLOHEXYLIODOMETHANE

(IODOMETHYL)CYCLOHEXANE

Cyclohexane, (iodoMethyl)-

Benzo[b]thiophene-2-carboxylicacid,5,8-dimethoxy-,methylester

5469-33-0

C6H11CH2I

C7H13I