ChemicalBook > CAS DataBase List > 3-FLUORO-4-IODOTOLUENE

3-FLUORO-4-IODOTOLUENE

Product Name: 3-FLUORO-4-IODOTOLUENE
CAS No.: 452-79-9
Chemical Name: 3-FLUORO-4-IODOTOLUENE
Synonyms: BUTTPARK 148\01-16;3-FLUORO-4-IODOTOLUENE;4-IODO-3-FLUOROTOLUENE;Benzene, 2-fluoro-1-iodo-4-methyl-;3-FLUORO-4-IODOTOLUENE ISO 9001：2015 REACH
CBNumber: CB4730262
Molecular Formula: C7H6FI
Formula Weight: 236.03
MOL File: 452-79-9.mol

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3-FLUORO-4-IODOTOLUENE Property

Boiling point:: 138-139 °C/9 mmHg (lit.)
Density: 1.803 g/mL at 25 °C (lit.)
refractive index: n20/D 1.5810(lit.)
Flash point:: 199 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
Appearance: Pink to red Liquid
Sensitive: Light Sensitive
CAS DataBase Reference: 452-79-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 52/53
Safety Statements: 23-24/25-61-60
WGK Germany: 3
Hazard Note: Irritant
HS Code: 29039990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H402Harmful to aquatic life

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P403+P235Store in a well-ventilated place. Keep cool.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 635154
Product name: 3-Fluoro-4-iodotoluene
Purity: 97%
Packaging: 1g
Price: $45.6
Updated: 2023/06/20

Sigma-Aldrich

Product number: 635154
Product name: 3-Fluoro-4-iodotoluene
Purity: 97%
Packaging: 5g
Price: $136
Updated: 2023/06/20

TRC

Product number: F632328
Product name: 3-Fluoro-4-Iodotoluene
Packaging: 500mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 6242AB
Product name: 3-Fluoro-4-iodotoluene
Packaging: 1g
Price: $14
Updated: 2021/12/16

Apolloscientific

Product number: PC8202
Product name: 3-Fluoro-4-iodotoluene
Packaging: 1g
Price: $15
Updated: 2021/12/16

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3-FLUORO-4-IODOTOLUENE Chemical Properties,Usage,Production

Chemical Properties

colorless to light yellow liqui

Synthesis

452-74-4

452-79-9

A solution was prepared by dissolving 4-bromo-3-fluorotoluene (10 g) in tetrahydrofuran (THF, 50 mL) under a dry nitrogen atmosphere and cooled to -72 °C. Subsequently, a hexane solution (35 mL) of 1.6 M n-butyllithium was slowly added at -72 °C, the reaction temperature was controlled not to exceed -65 °C and stirring was continued for 1 h at this temperature. A solution prepared by dissolving iodine (14.8 g) in THF (30 mL) was added to the above reaction mixture at -72 °C, ensuring that the internal temperature was not higher than -60 °C, after which it was slowly warmed to room temperature. Upon completion of the reaction, saturated aqueous ammonium chloride solution and hexane were added to the mixture to separate the organic layer. The organic layer was sequentially washed twice with 10% aqueous sodium sulfite, then with saturated brine and finally dried with anhydrous sodium sulfate. The desiccant was removed by filtration and the organic solvent was removed by distillation under reduced pressure. The residue was purified by silica gel column chromatography to give 13.0 g of 3-fluoro-4-iodotoluene as a yellow liquid.

References

[1] Patent: US2014/275577, 2014, A1. Location in patent: Paragraph 0166; 0167

3-FLUORO-4-IODOTOLUENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-FLUORO-4-IODOTOLUENE manufacturers

Henan Fengda Chemical Co., Ltd

Product: 3-FLUORO-4-IODOTOLUENE 452-79-9
Price: US $101.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-28

Career Henan Chemical Co

Product: 3-FLUORO-4-IODOTOLUENE 452-79-9
Price: US $2.00/KG
Min. Order: 1KG
Purity: 98%MIN
Supply Ability: ASK
Release date: 2019-12-25

452-79-9, 3-FLUORO-4-IODOTOLUENERelated Search:

Benzonitrile 4-IODO-2,3-DIFLUOROBENZOIC ACID 3-FLUORO-4-IODOTOLUENE 4-Fluoro-2-iodotoluene 98%,4-Fluoro-2-iodotoluene98%,4-FLUORO-2-IODOTOLUENE 3-FLUORO-2-IODOTOLUENE 4-FLUORO-3-IODOTOLUENE 3-FLUORO-5-IODOTOLUENE,5-Fluoro-3-iodotoluene,3-Fluoro-5-iodotoluene98% 2-FLUORO-4-IODOTOLUENE,2-Fluoro-4-iodotoluene,99%,2-Fluoro-4-iodotoluene 98%,2-Fluoro-4-iodotoluene98% 4-Iodotoluene difluoride 5-FLUORO-2-IODOTOLUENE, 97% MIN.,5-FLUORO-2-IODOTOLUENE,3-FLUORO-6-IODOTOLUENE 2-Fluoro-3-iodotoluene 2-Fluoro-5-iodotoluene 99%,2-FLUORO-5-IODOTOLUENE,2-Fluoro-5-iodotoluene,99% 2-FLUORO-6-IODOTOLUENE 3-Bromo-5-fluoro-2-iodotoluene 4-Iodotoluene 3-FLUORO-4-IODOBENZOTRIFLUORIDE 3-Bromo-5-fluoro-4-iodotoluene 3-FLUORO-4-IODOBENZALDEHYDE

BUTTPARK 148\01-16

4-IODO-3-FLUOROTOLUENE

3-FLUORO-4-IODOTOLUENE

Benzene, 2-fluoro-1-iodo-4-methyl-

3-FLUORO-4-IODOTOLUENE ISO 9001：2015 REACH

452-79-9

IC6H3FCH3

Building Blocks

Aryl

Halogenated Hydrocarbons

Organic Building Blocks

Fluorine Compounds

Iodine Compounds

Aryl

Halogenated Hydrocarbons

Aromatic Halides (substituted)

Halogen toluene

Fluoro-contained Iodo series