2,5-DIBROMO-3-CHLOROPYRIDINE
- Product Name
- 2,5-DIBROMO-3-CHLOROPYRIDINE
- CAS No.
- 160599-70-2
- Chemical Name
- 2,5-DIBROMO-3-CHLOROPYRIDINE
- Synonyms
- 2,5-Dibromo-3-chL;5-dibroMo-3-chloropyridine;2,5-DIBROMO-3-CHLOROPYRIDINE;2,5-DibroMo-3-chloropyrid...;3-Chloro-2,5-dibromopyridine;Pyridine, 2,5-dibromo-3-chloro-;2,5-DIBROMO-3-CHLOROPYRIDINE ISO 9001:2015 REACH
- CBNumber
- CB4739159
- Molecular Formula
- C5H2Br2ClN
- Formula Weight
- 271.34
- MOL File
- 160599-70-2.mol
2,5-DIBROMO-3-CHLOROPYRIDINE Property
- Boiling point:
- 263.3±35.0 °C(Predicted)
- Density
- 2.136±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -3.85±0.20(Predicted)
- form
- powder
- color
- Off-white
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D425820
- Product name
- 2,5-Dibromo-3-chloropyridine
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 3H32-D-81
- Product name
- 2,5-Dibromo-3-chloropyridine
- Packaging
- 5G
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FC08150
- Product name
- 3-Chloro-2,5-dibromopyridine
- Packaging
- 2g
- Price
- $64
- Updated
- 2021/12/16
- Product number
- FC08150
- Product name
- 3-Chloro-2,5-dibromopyridine
- Packaging
- 5G
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 069695
- Product name
- 2,5-Dibromo-3-chloropyridine
- Purity
- 97%
- Packaging
- 25g
- Price
- $144
- Updated
- 2021/12/16
2,5-DIBROMO-3-CHLOROPYRIDINE Chemical Properties,Usage,Production
Uses
2,5-Dibromo-3-chloropyridine is used in organic synthesis and pharmaceutical research.
Synthesis
97966-00-2
160599-70-2
General procedure for the synthesis of 2,5-dibromo-3-chloropyridine from 5-bromo-2,3-dichloropyridine: To 5-bromo-2,3-dichloropyridine (11.7 g, 51.6 mmol) was added 5 M hydrobromic acid solution of acetic acid (51.6 mL, 258 mmol) at room temperature. The reaction mixture was then heated to 70 °C and kept stirring for 7 hours. Upon completion of the reaction, the reaction mixture was diluted with ethyl acetate, the reaction was quenched with water and extracted with ethyl acetate. The organic layers were combined, washed with 1 M sodium hydroxide solution, dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure. The residue was recrystallized by hexane-ethyl acetate mixed solvent to give 11.2 g of the target product 2,5-dibromo-3-chloropyridine in 80% yield as a white solid.1H-NMR (DMSO-d6) δ: 8.55 (1H, s), 8.49 (1H, s).
References
[1] Patent: US9156830, 2015, B2. Location in patent: Page/Page column 104
2,5-DIBROMO-3-CHLOROPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,5-DIBROMO-3-CHLOROPYRIDINE manufacturers
- Product
- 2,5-DIBROMO-3-CHLOROPYRIDINE 160599-70-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-06-03
- Product
- 2,5-DIBROMO-3-CHLOROPYRIDINE 160599-70-2
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
- Product
- 2,5-DIBROMO-3-CHLOROPYRIDINE 160599-70-2
- Price
- US $20.00/kg
- Min. Order
- 1kg
- Purity
- 99.99%
- Supply Ability
- 50000tons
- Release date
- 2023-08-08