synthesis
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5-NITROBARBITURIC ACID

synthesis
Product Name
5-NITROBARBITURIC ACID
CAS No.
480-68-2
Chemical Name
5-NITROBARBITURIC ACID
Synonyms
AKOS 89968;AURORA KA-3829;DILITURIC ACID;5-Nitrobarbitursαure;NITROBARBITURIC ACID;5-Nitrobarbiuricacid;5-nitro-barbituricaci;5-NITROBARBITURIC ACID;5-Nitrobarbituric Acid 5-NITROPRIMIDINE-2,4,6-TRIOL
CBNumber
CB4777748
Molecular Formula
C4H3N3O5
Formula Weight
173.08
MOL File
480-68-2.mol
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5-NITROBARBITURIC ACID Property

Melting point:
180.5°C
Boiling point:
303.69°C (rough estimate)
Density 
1.79±0.1 g/cm3(Predicted)
refractive index 
1.5000 (estimate)
storage temp. 
Store at -20°C
pka
-1.70±0.20(Predicted)
form 
Solid
color 
Off-white to light yellow
Merck 
6585
CAS DataBase Reference
480-68-2(CAS DataBase Reference)
EPA Substance Registry System
2,4,6(1H,3H,5H)-Pyrimidinetrione, 5-nitro- (480-68-2)
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36/37/39-36
RTECS 
CQ7300000
HazardClass 
IRRITANT
HS Code 
29335400
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
N900978
Product name
5-NitrobarbituricAcid
Packaging
25g
Price
$175
Updated
2021/12/16
Matrix Scientific
Product number
058112
Product name
5-Nitropyrimidine-2,4,6(1H,3H,5H)-trione
Purity
95%
Packaging
25g
Price
$240
Updated
2021/12/16
ChemScene
Product number
CS-W002008
Product name
5-Nitropyrimidine-2,4,6(1H,3H,5H)-trione
Purity
≥97.0%
Packaging
100g
Price
$254
Updated
2021/12/16
ChemScene
Product number
CS-W002008
Product name
5-Nitropyrimidine-2,4,6(1H,3H,5H)-trione
Purity
≥97.0%
Packaging
25g
Price
$74
Updated
2021/12/16
Matrix Scientific
Product number
058112
Product name
5-Nitropyrimidine-2,4,6(1H,3H,5H)-trione
Purity
95%
Packaging
5g
Price
$140
Updated
2021/12/16
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5-NITROBARBITURIC ACID Chemical Properties,Usage,Production

synthesis

5-Nitrobarbituric acid can be obtained by nitration of barbituric acid with fuming nitric acid below 40°C with a yield of 85-90%.

Chemical Properties

Prisms and leaflets from water.Slightly soluble in water; soluble in alcohol and sodium hydroxide solution; insoluble in ether.

Uses

Microreagent for potassium.

Purification Methods

Crystallise diliuric acid from water as the trihydrate (m 180-181o (dec). Drying over 70% H2SO4 converts the trihydrate to the dihydrate [Loeffler & Moore J Am Chem Soc 70 3650 1948]. [Beilstein 24 H 474, 24 II 273, 24 III/IV 1882.]

5-NITROBARBITURIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-NITROBARBITURIC ACID manufacturers

Apeloa production Co.,Limited
Product
5-Nitrobarbituric acid 480-68-2
Price
US $1.00/g
Min. Order
1g
Purity
0.98
Supply Ability
1000
Release date
2024-07-19
Shaanxi Dideu Medichem Co. Ltd
Product
5-NITROBARBITURIC ACID 480-68-2
Price
US $1.00-100.00/KG
Min. Order
1KG
Purity
95%
Supply Ability
300KG
Release date
2024-08-19
Henan Aochuang Chemical Co.,Ltd.
Product
5-NITROBARBITURIC ACID 480-68-2
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1Ton
Release date
2022-09-22

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