1,8-Dibromopyrene
- Product Name
- 1,8-Dibromopyrene
- CAS No.
- 38303-35-4
- Chemical Name
- 1,8-Dibromopyrene
- Synonyms
- 1,8-Dibromopyrene;Pyrene, 1,8-dibromo-
- CBNumber
- CB4948315
- Molecular Formula
- C16H8Br2
- Formula Weight
- 360.04
- MOL File
- 38303-35-4.mol
1,8-Dibromopyrene Property
- Melting point:
- 211 °C
- Boiling point:
- 469.6±18.0 °C(Predicted)
- Density
- 1.852±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to light yellow Solid
- InChI
- InChI=1S/C16H8Br2/c17-13-7-3-9-1-2-10-4-8-14(18)12-6-5-11(13)15(9)16(10)12/h1-8H
- InChIKey
- JBLQSCAVCHTKPV-UHFFFAOYSA-N
- SMILES
- C1(Br)=C2C3=C4C(C=C2)=C(Br)C=CC4=CC=C3C=C1
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D3168
- Product name
- 1,8-Dibromopyrene
- Packaging
- 200MG
- Price
- $83
- Updated
- 2025/07/31
- Product number
- D3168
- Product name
- 1,8-Dibromopyrene
- Packaging
- 1G
- Price
- $346
- Updated
- 2023/01/07
- Product number
- HCH0115595
- Product name
- 1,8-DIBROMOPYRENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.65
- Updated
- 2021/12/16
- Product number
- FD150457
- Product name
- 1,8-Dibromopyrene
- Packaging
- 1g
- Price
- $550
- Updated
- 2021/12/16
- Product number
- FD150457
- Product name
- 1,8-Dibromopyrene
- Packaging
- 100mg
- Price
- $91
- Updated
- 2021/12/16
1,8-Dibromopyrene Chemical Properties,Usage,Production
Synthesis
129-00-0
27973-29-1
38303-35-4
The general procedure for the synthesis of 1,6-dibromopyrene and 1,8-dibromopyrene from pyrene was as follows: first, 58 g (0.287 mol) of pyrene was dissolved in 1750 ml of chloroform. Subsequently, 31 ml (0.609 mol) of bromine in 250 ml of chloroform was slowly added dropwise at room temperature and protected from light. After the dropwise addition was completed, the reaction mixture was heated under reflux conditions for 4 hours. After completion of the reaction, the mixture was cooled and the precipitated solid product was collected by diafiltration. The solid was washed with ethanol to remove impurities and then dried. Finally, the solid obtained was recrystallized from chloroform three times to improve the purity of the product. Ultimately, 73.4 g (0.201 mol) of 1,6-dibromopyrene was obtained in 71.1% yield of the theoretical value, as well as 20.6 g (0.06 mol) of 1,8-dibromopyrene in 20% yield of the theoretical value.
References
[1] Dyes and Pigments, 2016, vol. 130, p. 106 - 115
[2] Journal of Molecular Structure, 2017, vol. 1127, p. 237 - 246
[3] Patent: WO2013/185871, 2013, A1. Location in patent: Page/Page column 24
[4] Mendeleev Communications, 2016, vol. 26, # 5, p. 437 - 439
[5] Dyes and Pigments, 2018, vol. 158, p. 42 - 49
1,8-Dibromopyrene Preparation Products And Raw materials
Raw materials
Preparation Products
1,8-Dibromopyrene Suppliers
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View Lastest Price from 1,8-Dibromopyrene manufacturers
- Product
- 1,8-Dibromopyrene 38303-35-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-16
- Product
- 1,8-Dibromopyrene 38303-35-4
- Price
- US $600.00-20000.00/KG
- Min. Order
- 1g
- Purity
- 98
- Supply Ability
- 100kg
- Release date
- 2019-05-23
- Product
- 1,8-Dibromopyrene 38303-35-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 20KG
- Release date
- 2018-08-07