2-Methoxy-6-fluorobenzyl cyanide

Product Name: 2-Methoxy-6-fluorobenzyl cyanide
CAS No.: 500912-18-5
Chemical Name: 2-Methoxy-6-fluorobenzyl cyanide
Synonyms: 2-Fluoro-6-Methoxybenzyl cyanide;2-Fluoro-6-methoxybenzeneacetonitrile;2-(2-Fluoro-6-Methoxyphenyl)acetonitrile;Benzeneacetonitrile, 2-fluoro-6-methoxy-;2-fluoro-2-(2-methoxyphenyl)acetonitrile;2-Fluoro-6-methoxyphenylacetonitrile 95+%;Benzeneacetonitrile, 2-fluoro-6-methoxy- (9CI);2-Fluoro-6-methoxybenzyl cyanide, 2-(Cyanomethyl)-3-fluoroanisole
CBNumber: CB4971759
Molecular Formula: C9H8FNO
Formula Weight: 165.16
MOL File: 500912-18-5.mol

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2-Methoxy-6-fluorobenzyl cyanide Property

Boiling point:: 239℃
Density: 1.148
Flash point:: 99℃
storage temp.: Sealed in dry,Room Temperature
form: liquid
color: Colourless

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: F599368
Product name: 2-Fluoro-6-methoxybenzylCyanide
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: F599368
Product name: 2-Fluoro-6-methoxybenzylCyanide
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Apolloscientific

Product number: PC0905
Product name: 2-Fluoro-6-methoxyphenylacetonitrile
Purity: 95+%
Packaging: 1g
Price: $85
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4637-3-T3
Product name: 2-Fluoro-6-methoxyphenylacetonitrile
Packaging: 1g
Price: $93
Updated: 2021/12/16

AK Scientific

Product number: 6831AB
Product name: 2-(2-Fluoro-6-methoxyphenyl)acetonitrile
Packaging: 250mg
Price: $117
Updated: 2021/12/16

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2-Methoxy-6-fluorobenzyl cyanide Chemical Properties,Usage,Production

Synthesis

773837-37-9

146137-74-8

500912-18-5

General procedure for the synthesis of 2-fluoro-6-methoxyphenylacetonitrile from the compound (CAS: 773837-37-9) and 2-fluoro-6-methoxybenzaldehyde: Sodium cyanide (1.4 g, 28.76 mmol) was added to a solution of compound 3 (5.7 g, 26.15 mmol) in anhydrous ethanol (70 mL) and the reaction mixture was stirred at 80 °C for 4 hour. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the complete consumption of the raw materials, the reaction mixture was concentrated to obtain the crude product. The crude product was diluted with ice water (30 mL) and extracted with ethyl acetate (2 x 50 mL). The organic layers were combined, washed with brine (20 mL), dried over anhydrous sodium sulfate and concentrated to give the residue. The residue was purified by column chromatography with the eluent of petroleum ether/ethyl acetate (initial ratio 100/0, gradually increased to 60/40) to afford compound 4 (2.0 g, 46% yield) as a colorless liquid. The mass spectrum (ESI) showed the molecular ion peak [M+H]+ = 166.06.

References

[1] Patent: WO2014/52365, 2014, A1. Location in patent: Page/Page column 299-300

2-Methoxy-6-fluorobenzyl cyanide Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Methoxy-6-fluorobenzyl cyanide Suppliers

China 30 Europe 1 Germany 1 India 1 Italy 1 United Kingdom 2 United States 5 Global 41

Beijing Eternalchem Co,. Ltd.

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500912-18-5, 2-Methoxy-6-fluorobenzyl cyanideRelated Search:

Benzeneacetonitrile 2-Methoxyphenylacetonitrile 2-Fluorobenzyl cyanide (S)-10-(Cyanomethyl)-9-fluoro-2,3-dihydro-3-methyl-7-oxo-7H-pyrido[1,2,3-de]-1,4-benzoxazine-6-carboxylic acid 2-Methoxy-6-fluorobenzyl cyanide 2,3-DIFLUORO-6-METHOXYPHENYLACETONITRILE

Benzeneacetonitrile, 2-fluoro-6-methoxy- (9CI)

2-Fluoro-6-methoxybenzeneacetonitrile

2-Fluoro-6-Methoxybenzyl cyanide

2-(2-Fluoro-6-Methoxyphenyl)acetonitrile

2-Fluoro-6-methoxybenzyl cyanide, 2-(Cyanomethyl)-3-fluoroanisole

2-Fluoro-6-methoxyphenylacetonitrile 95+%

2-fluoro-2-(2-methoxyphenyl)acetonitrile

Benzeneacetonitrile, 2-fluoro-6-methoxy-

500912-18-5

Fluorine series

HALIDE

METHOXY