Pyrimidine, 4-(chloromethyl)- (9CI)
- Product Name
- Pyrimidine, 4-(chloromethyl)- (9CI)
- CAS No.
- 54198-81-1
- Chemical Name
- Pyrimidine, 4-(chloromethyl)- (9CI)
- Synonyms
- 4-pyriMidinylMethyl chloride;PyriMidine, 4-(chloroMethyl)-;Pyrimidine, 4-(chloromethyl)- (9CI)
- CBNumber
- CB51046387
- Molecular Formula
- C5H5ClN2
- Formula Weight
- 128.5596
- MOL File
- 54198-81-1.mol
Pyrimidine, 4-(chloromethyl)- (9CI) Property
- Boiling point:
- 219℃
- Density
- 1.241
- Flash point:
- 107℃
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H314Causes severe skin burns and eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B423905
- Product name
- 4-(chloromethyl)pyrimidine
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- HCH0366201
- Product name
- 4-(CHLOROMETHYL)PYRIMIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.41
- Updated
- 2021/12/16
- Product number
- A243131
- Product name
- 4-(Chloromethyl)pyrimidine
- Purity
- 97%
- Packaging
- 250mg
- Price
- $106
- Updated
- 2021/12/16
- Product number
- CM337732
- Product name
- 4-(Chloromethyl)pyrimidine
- Purity
- 95%+
- Packaging
- 100mg
- Price
- $156
- Updated
- 2021/12/16
- Product number
- CM337732
- Product name
- 4-(Chloromethyl)pyrimidine
- Purity
- 95%+
- Packaging
- 250mg
- Price
- $260
- Updated
- 2021/12/16
Pyrimidine, 4-(chloromethyl)- (9CI) Chemical Properties,Usage,Production
Synthesis
3438-46-8
94-36-0
54198-81-1
The general procedure for the synthesis of 4-(chloromethyl)pyrimidine was as follows: a mixture of 4-methylpyrimidine (2 g, 21.2 mmol), N-chlorosuccinimide (4.26 g, 31.9 mmol), and dibenzoyl peroxide (500 mg) in carbon tetrachloride (100 ml) was heated to 80°C and maintained at this temperature for 2 hours of reaction. After completion of the reaction, the mixture was cooled to room temperature and subsequently filtered. The filtrate was concentrated under reduced pressure to remove the solvent and the crude product was obtained as an oil. The oil was purified by fast column chromatography using dichloromethane as eluent to give 4-(chloromethyl)pyrimidine as an orange oil (1 g, 37% yield).
References
[1] Patent: US5962458, 1999, A
Pyrimidine, 4-(chloromethyl)- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Pyrimidine, 4-(chloromethyl)- (9CI) manufacturers
- Product
- 4-ChloroMethyl-pyriMidine 54198-81-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2020-05-15