ChemicalBook > CAS DataBase List > BUTTPARK 146\18-29

BUTTPARK 146\18-29

Product Name
BUTTPARK 146\18-29
CAS No.
108831-66-9
Chemical Name
BUTTPARK 146\18-29
Synonyms
BUTTPARK 146\18-29;6-Methylthieno[2,3-d]Pyrimid-4-One;6-METHYLTHIENO[2,3-D]PYRIMIDIN-4-OL;BUTTPARK 146\18-29 ISO 9001:2015 REACH;6-Methyl-1H-thieno[2,3-d]pyrimidin-4-one;6-methyl-3H-thieno[3,2-e]pyrimidin-4-one;6-Methylthieno[2,3-d]pyrimidin-4(3H)-one;3-Phenyl-4,5-dihydro-[1,2,4]oxadiazol-5-ol;6-Methyl-3H,4H-thieno[2,3-d]pyriMidin-4-one;Thieno[2,3-d]pyrimidin-4(1H)-one, 6-methyl-
CBNumber
CB5104794
Molecular Formula
C7H6N2OS
Formula Weight
166.2
MOL File
108831-66-9.mol
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BUTTPARK 146\18-29 Property

Melting point:
195-200℃ (ethanol )
Boiling point:
406.7±33.0 °C(Predicted)
Density 
1.53±0.1 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
11.56±0.20(Predicted)
Appearance
Off-white to light brown Solid
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Safety

Risk Statements 
20/21/22
Safety Statements 
3/7-36/37
HS Code 
29335990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Frontier Specialty Chemicals
Product number
JK182970
Product name
6-Methyl-3H-thieno[2,3-d]pyrimidin-4-one
Purity
97%
Packaging
1g
Price
$43
Updated
2021/12/16
Apolloscientific
Product number
OR932092
Product name
6-Methylthieno[2,3-d]pyrimidin-4-ol
Purity
95%
Packaging
1g
Price
$95
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
JK182970
Product name
6-Methyl-3H-thieno[2,3-d]pyrimidin-4-one
Purity
97%
Packaging
5g
Price
$163
Updated
2021/12/16
Matrix Scientific
Product number
077382
Product name
6-Methylthieno[2,3-d]pyrimidin-4(3H)-one
Packaging
500mg
Price
$168
Updated
2021/12/16
Apolloscientific
Product number
OR932092
Product name
6-Methylthieno[2,3-d]pyrimidin-4-ol
Purity
95%
Packaging
5g
Price
$200
Updated
2021/12/16
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BUTTPARK 146\18-29 Chemical Properties,Usage,Production

Chemical Properties

Yellow solid

Synthesis

4815-32-1

77287-34-4

108831-66-9

General procedure for the synthesis of 6-methyl-3H-thieno[2,3-d]pyrimidin-4-one from ethyl 2-amino-5-methylthiophene-3-carboxylate (2.3 g, 12.0 mmol) and formamide (28 mL): a suspension of ethyl 2-amino-5-methylthiophene-3-carboxylate and formamide was heated and reacted for 16 hours at 180 °C. Upon completion of the reaction, the reaction mixture was quenched with 100 mL of water and stirring was continued for 30 minutes. The precipitated solid was collected by filtration, washed with pentane and dried by filtration to give 6-methyl-3H-thieno[2,3-d]pyrimidin-4-one (1.0 g, crude) as an off-white solid. Results of mass spectrometry analysis: calculated value (M + H): 167.02; measured value (M + H): 167.1.

References

[1] Pharmaceutical Chemistry Journal, 1987, vol. 21, # 2, p. 126 - 129
[2] Khimiko-Farmatsevticheskii Zhurnal, 1987, vol. 21, # 2, p. 197 - 200
[3] European Journal of Medicinal Chemistry, 2011, vol. 46, # 3, p. 870 - 876
[4] European Journal of Medicinal Chemistry, 2016, vol. 115, p. 148 - 160
[5] Patent: WO2017/100599, 2017, A1. Location in patent: Paragraph 00125-00126

BUTTPARK 146\18-29 Preparation Products And Raw materials

Raw materials

Preparation Products

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BUTTPARK 146\18-29 Suppliers

Specs
Tel
--
Fax
--
Email
info@specs.net
Country
The Netherlands
ProdList
6833
Advantage
70
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View Lastest Price from BUTTPARK 146\18-29 manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
BUTTPARK 146\18-29 108831-66-9
Price
US $1.10/g
Min. Order
1g
Purity
99.0% min
Supply Ability
100 tons min
Release date
2021-05-13