ChemicalBook > CAS DataBase List > Phenylsulfenylchloride
Phenylsulfenylchloride
- Product Name
- Phenylsulfenylchloride
- CAS No.
- 931-59-9
- Chemical Name
- Phenylsulfenylchloride
- Synonyms
- phenyl hypochlorothioite;fenyL;BENZENESULFENYL CHLORIDE;(Chlorothio)benzene;Phenylthio chloride;Phenylchloro sulfide;Phenylsulfenylchloride;Benzene, (chlorothio)-;Phenyl Thiohypochlorite;(Chlorosulfanyl)benzene
- CBNumber
- CB51075374
- Molecular Formula
- C6H5ClS
- Formula Weight
- 144.62
- MOL File
- 931-59-9.mol
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Phenylsulfenylchloride Property
- Boiling point:
- 262℃
- Density
- 1.25
- Flash point:
- 110℃
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
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N-Bromosuccinimide Price
TRC
- Product number
- P296045
- Product name
- PhenylsulfenylChloride
- Packaging
- 25mg
- Price
- $90
- Updated
- 2021/12/16
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Phenylsulfenylchloride Chemical Properties,Usage,Production
Uses
Phenylsulfenyl Chloride is an intermediate used in the synthesis of Tabanone (T003450), which is found in oils of Trifolium pratense L. and is a potential natural anti-oxidant.
Preparation
To a flask containing 32.7 gm (0.15 mole) of diphenyl disulfide dissolved in 100 ml of dichloromethane containing 3 ml of pyridine is slowly dropwise added at room temperature 20.3 gm (0.15 mole) of freshly distilled sulfuryl chloride. After completion of the addition, the solution is stirred for an additional hour, concentrated under reduced pressure (12 mm Hg) at 25°C, and the residue distilled to afford 33 gm (76%), b.p. 49°C (4 mm Hg), of a dark red liquid.
Synthesis Reference(s)
The Journal of Organic Chemistry, 43, p. 1208, 1978 DOI: 10.1021/jo00400a041
Chemical and Pharmaceutical Bulletin, 28, p. 126, 1980 DOI: 10.1248/cpb.28.126
Phenylsulfenylchloride Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Phenylsulfenylchloride manufacturers
Zhuozhou Wenxi import and Export Co., Ltd
- Product
- Benzenesulfenyl chloride 931-59-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
- Product
- Benzenesulfenyl chloride 931-59-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-08
Shaanxi Dideu Medichem Co. Ltd
- Product
- Phenylsulfenylchloride 931-59-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2020-01-07