ChemicalBook > CAS DataBase List > 2,4-Dibromo-1-nitrobenzene

2,4-Dibromo-1-nitrobenzene

Product Name
2,4-Dibromo-1-nitrobenzene
CAS No.
51686-78-3
Chemical Name
2,4-Dibromo-1-nitrobenzene
Synonyms
2,4-Dibromo-1-nitrobenzene;1,3-Dibromo-4-nitrobenzene;4-Dibromonitrobenzene;2,4-Dibromonitrobenzene;,3-Dibromo-4-nitrobenzene;2,4-Dibromo-1-nitrobenzene>Benzene, 2,4-dibroMo-1-nitro-;1,3-Dibromo-4-nitrobenzene,98%;2,4-Dibromonitrobenzene 51686-78-3
CBNumber
CB51095608
Molecular Formula
C6H3Br2NO2
Formula Weight
280.9
MOL File
51686-78-3.mol
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2,4-Dibromo-1-nitrobenzene Property

Melting point:
61-62℃
Boiling point:
270℃
Density 
2.101
refractive index 
1.6400 (estimate)
Flash point:
117℃
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
Crystalline Powder
color 
Yellow
InChIKey
DXRVYZGVVFZCFP-UHFFFAOYSA-N
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Safety

HS Code 
2904.99.4700
HazardClass 
6.1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D4790
Product name
2,4-Dibromo-1-nitrobenzene
Purity
>98.0%(GC)
Packaging
1g
Price
$20
Updated
2024/03/01
TCI Chemical
Product number
D4790
Product name
2,4-Dibromo-1-nitrobenzene
Purity
>98.0%(GC)
Packaging
5g
Price
$51
Updated
2024/03/01
Alfa Aesar
Product number
H61738
Product name
1,3-Dibromo-4-nitrobenzene, 98%
Packaging
1g
Price
$131
Updated
2021/12/16
Alfa Aesar
Product number
H61738
Product name
1,3-Dibromo-4-nitrobenzene, 98%
Packaging
5g
Price
$521
Updated
2021/12/16
Alfa Aesar
Product number
H61738
Product name
1,3-Dibromo-4-nitrobenzene, 98%
Packaging
250mg
Price
$43.8
Updated
2021/12/16
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2,4-Dibromo-1-nitrobenzene Chemical Properties,Usage,Production

Description

2,4-Dibromo-1-nitrobenzene is a pharmaceutical intermediate that can be obtained by nitration of m-dibromobenzene. This compound can be used to prepare the benzimidazole anthelmintic fenbendazole through a four-step reaction.

Chemical Properties

Light yellow powder

Production Methods

Dissolve 24.5g of m-dibromobenzene in 49.0g of concentrated sulfuric acid (98%) at room temperature, cool to 0-5°C, add 9.80g of nitric acid (68%) dropwise, control the temperature at 0-5°C during the addition process, and stir at 5-10°C for 2 hours after the addition is complete. After the reaction is completed, add the reaction solution dropwise to 49.0g of cold water, and the temperature does not exceed 60°C during the quenching process. After the quenching is completed, stir at room temperature for 0.5 hours, filter, and wash the filter cake with 15.0g of water to obtain 31.95g (water content 16.0%) of 2,4-Dibromo-1-nitrobenzene tide product with a purity of 99.75%.

2,4-Dibromo-1-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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2,4-Dibromo-1-nitrobenzene Suppliers

3B Pharmachem (Wuhan) International Co.,Ltd.
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View Lastest Price from 2,4-Dibromo-1-nitrobenzene manufacturers

Career Henan Chemical Co
Product
2,4-Dibromonitrobenzene 51686-78-3
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2019-12-30