2-(1-Cyclohexenyl)ethylamine
- Product Name
- 2-(1-Cyclohexenyl)ethylamine
- CAS No.
- 3399-73-3
- Chemical Name
- 2-(1-Cyclohexenyl)ethylamine
- Synonyms
- CYCLOHEXENYLETHYLAMINE;2-(Cyclohex-1-en-1-yl)ethanamine;ohexenyL;2-(1-CycL;RARECHEM AN KA 1280;cyclohexenethylamine;2-Cyclohexenyl ethylamine;Cyclohexen-1-ylethylamine;2-AMINOETHYL-1-CYCLOHEXENE;1-CYCLOHEXENE-2-ETHANAMINE
- CBNumber
- CB5112809
- Molecular Formula
- C8H15N
- Formula Weight
- 125.21
- MOL File
- 3399-73-3.mol
2-(1-Cyclohexenyl)ethylamine Property
- Melting point:
- -55 °C
- Boiling point:
- 53-54 °C/2.5 mmHg (lit.)
- Density
- 0.898 g/mL at 25 °C (lit.)
- refractive index
- 1.486-1.488
- Flash point:
- 57 °C
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- pka
- 10.94±0.10(Predicted)
- form
- clear liquid
- color
- Colorless to Light yellow
- Sensitive
- Air Sensitive
- BRN
- 774030
- Stability:
- Light Sensitive
- InChIKey
- IUDMXOOVKMKODN-UHFFFAOYSA-N
- CAS DataBase Reference
- 3399-73-3(CAS DataBase Reference)
- EPA Substance Registry System
- 1-Cyclohexene-1-ethanamine (3399-73-3)
Safety
- Hazard Codes
- C
- Risk Statements
- 34
- Safety Statements
- 28A-26-45-36/37/39
- RIDADR
- 2735
- WGK Germany
- 3
- TSCA
- Yes
- HazardClass
- 8
- PackingGroup
- II
- HS Code
- 29213000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H226Flammable liquid and vapour
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233Keep container tightly closed.
P240Ground/bond container and receiving equipment.
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 255866
- Product name
- 2-(1-Cyclohexenyl)ethylamine
- Purity
- 97%
- Packaging
- 5g
- Price
- $72.3
- Updated
- 2023/01/07
- Product number
- C1157
- Product name
- 2-(1-Cyclohexenyl)ethylamine
- Purity
- >98.0%(GC)(T)
- Packaging
- 25mL
- Price
- $45
- Updated
- 2024/03/01
- Product number
- C1157
- Product name
- 2-(1-Cyclohexenyl)ethylamine
- Purity
- >98.0%(GC)(T)
- Packaging
- 500mL
- Price
- $284
- Updated
- 2024/03/01
- Product number
- C991470
- Product name
- 2-(1-Cyclohexenyl)ethylamine
- Packaging
- 1g
- Price
- $55
- Updated
- 2021/12/16
- Product number
- X6206
- Product name
- 2-(1-Cyclohexenyl)ethylamine
- Packaging
- 5g
- Price
- $111
- Updated
- 2021/12/16
2-(1-Cyclohexenyl)ethylamine Chemical Properties,Usage,Production
Chemical Properties
CLEAR COLOURLESS TO LIGHT YELLOW LIQUID
Uses
2-(1-Cyclohexenyl)ethylamine has been employed:
- as substrate for allylic hydroxylation reaction
- in preparation of thin films and single crystals of 2-(1-cyclohexenyl)ethyl ammonium lead iodide, used to fabricate optoelectronic-compatible heterostructures
Synthesis
125 ml of ethylamine was placed in a 250 ml three-necked flask, which had previously been flushed with argon, at -70 ° C. 6.27 g (50 mmol) of 2-phenylethylamine was added. The resulting clear, colorless solution was metered in with 1.14 g (164.2 mmol) of Li powder; the solution turned dark blue 5 minutes after the onset of turbidity. After stirring for 2 hours at -70 ° C, the mixture was warmed to -30 ° C. Then another 0.24 g (34.6 mmol) of Li powder was added. After stirring again at -30 ° C. for 2 hours, the cooling bath was removed. The reaction mixture was allowed to warm to room temperature overnight. The reaction mixture was then given 25 ml of abs. After that, a gray suspension formed. After stirring for 20 minutes at room temperature, 25 ml of water was slowly added (exothermic temperature 40 ° C.). The excess ethylamine was then distilled off at 40 °C. The distillation residue was evaporated to dryness. Then, 100 ml of water was added and extracted 3 times with 80 ml chloroform. The combined organic phases were dried over Na?SO?, filtered, and evaporated. The 2-(1-Cyclohexenyl)ethylamine was obtained in a GC yield of 69.8%.
2-(1-Cyclohexenyl)ethylamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(1-Cyclohexenyl)ethylamine manufacturers
- Product
- 2-(1-Cyclohexenyl)ethylamine 3399-73-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-07-19
- Product
- 2-(1-CYCLOHEXENYL)ETHYLAMINE 3399-73-3
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-12-17