ChemicalBook > CAS DataBase List > ETHINAMATE

ETHINAMATE

Product Name
ETHINAMATE
CAS No.
126-52-3
Chemical Name
ETHINAMATE
Synonyms
Valmid;Valamin;Volamin;Valamina;Ethinamat;Etinamate;usafel-42;Valmidate;ETHINAMATE;Ethinimate
CBNumber
CB5113169
Molecular Formula
C9H13NO2
Formula Weight
167.21
MOL File
126-52-3.mol
More
Less

ETHINAMATE Property

Melting point:
96-98°
Boiling point:
bp3 118-122°
Density 
1.1222 (rough estimate)
refractive index 
nD21.5 1.4441 (20% in propylene glycol)
solubility 
Chloroform (Slightly), Methanol (Slightly)
pka
13.40±0.50(Predicted)
EPA Substance Registry System
Cyclohexanol, 1-ethynyl-, carbamate (126-52-3)
More
Less

Safety

Hazard Codes 
T,Xn
Risk Statements 
23/24/25-22
Safety Statements 
22-36/37/39-45
RTECS 
GV9275000
Hazardous Substances Data
126-52-3(Hazardous Substances Data)
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

P501Dispose of contents/container to..…

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
E3258
Product name
Ethinamate
Purity
analytical standard
Packaging
100mg
Price
$168
Updated
2022/05/15
More
Less

ETHINAMATE Chemical Properties,Usage,Production

Originator

Valmid,Dista,US,1955

Uses

Ethinamate (E890730) is a an active central nervous system depressant used in the treatment of insomnia.

Definition

ChEBI: A carbamate ester that is the 1-vinylcyclohexyl ester of carbamic acid. A short-acting sedative-hypnotic, it was formerly used to treat insomnia.

Manufacturing Process

A solution of 34 cc (0.5 mol) of liquid phosgene in 150 cc of absolute ether is reacted while cooling with a mixture of sodium chloride and ice, first with 62 grams (0.5 mol) of 1-ethinyl cyclohexanol-1 and then with 64 cc (0.5 mol) of quinoline. The precipitated quinoline chlorohydrate is filtered off and the filtrate is reacted with ammonia in ether. In this manner 45 grams of the carbamic acid ester of 1-ethinyl cyclohexanol are obtained. Yield: 53% of the theoretical yield. The ester boils at 108° to 110°C/3 mm and on recrystallization from cyclohexane, yields colorless needles melting at 94° to 96°C.

Therapeutic Function

Sedative

Safety Profile

A deadly human poison. Experimental poison by ingestion, intravenous, subcutaneous, and intraperitoneal routes. An experimental teratogen. When heated to decomposition it emits toxic fumes of NOx. See also CARBAMATES.

ETHINAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

ETHINAMATE Suppliers

126-52-3, ETHINAMATERelated Search:


  • 1-ETHYNYLCYCLOHEXANOL CARBAMATE
  • ETHINAMATE
  • 1-Ethinylcyclohexyl carbamate
  • 1-ethinylcyclohexylcarbamate
  • 1-ethinylcyclohexylcarbonate
  • 1-ethynyl-cyclohexanocarbamate
  • 1-Ethynylcyclohexyl carbamate
  • 1-ethynylcyclohexylcarbamate
  • Aethinyl-cyclohexyl-carbamat
  • Carbamate de L'ethinylcyclohexanol
  • ethinamate--dea schedule iv item
  • GXRZIMHKGDIBEW-UHFFFAOYSA-N
  • carbamatedel’ethinylcyclohexanol
  • Carbamic acid, 1-ethynylcyclohexyl ester
  • carbamicacid,1-ethynylcyclohexylester
  • carbamicacid1-ethynylcyclohexylester
  • Cyclohexanol, 1-ethynyl-, carbamate
  • Ethinamat
  • Ethinimate
  • ethynylcyclohexylcarbamate
  • Etinamate
  • USAF el-42
  • usafel-42
  • Valamin
  • Valamina
  • valaminetta
  • Valaminettae
  • Valaminetten
  • Valmid
  • Valmidate
  • Volamin
  • Cyclohexanol, 1-ethynyl-, 1-carbamate
  • ETHINAMATE USP/EP/BP
  • 126-52-3
  • EQ - EZ
  • Analytical Standards
  • Alphabetic
  • Analytical Chromatography Product Catalog