4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE
- Product Name
- 4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE
- CAS No.
- 57341-98-7
- Chemical Name
- 4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE
- Synonyms
- BUTTPARK 46\04-33;4-Phenylethynyl-benzaldehyd;4-PHENYLETHYNYL-BENZALDEHYDE;4-(2-phenylethynyl)benzaldehyde;4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE;Benzaldehyde, 4-(2-phenylethynyl)-;Product English Name: 4-(Phenylethynyl)benzaldehyde
- CBNumber
- CB5124967
- Molecular Formula
- C15H10O
- Formula Weight
- 206.24
- MOL File
- 57341-98-7.mol
4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE Property
- Melting point:
- 102 °C
- Boiling point:
- 364.2±25.0 °C(Predicted)
- Density
- 1.14±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- crystalline solid
- color
- Light yellow
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2912290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P2975
- Product name
- 4-(Phenylethynyl)benzaldehyde
- Packaging
- 1G
- Price
- $89
- Updated
- 2025/07/31
- Product number
- P2975
- Product name
- 4-(Phenylethynyl)benzaldehyde
- Packaging
- 5G
- Price
- $267
- Updated
- 2025/07/31
- Product number
- B521363
- Product name
- 4-(Phenylethynyl)benzaldehyde
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- B521363
- Product name
- 4-(Phenylethynyl)benzaldehyde
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- P58124
- Product name
- 4-(Phenylethynyl)benzaldehyde
- Purity
- 97%
- Packaging
- 100mg
- Price
- $30
- Updated
- 2021/12/16
4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
87199-17-5
536-74-3
57341-98-7
4-Formylphenylboronic acid (0.5 mmol), phenylacetylene (0.6 mmol), dichloromethane (2 mL), Catalyst 3 (2 mol%), silver oxide (Ag2O, 1.0 mmol), and potassium acetate (KOAc, 1.0 mmol) were sequentially added to the Schlenk tube. The reaction mixture was stirred at 35 °C for 24 h under argon protection. Upon completion of the reaction, excess dichloromethane was removed by rotary evaporation and the residue was purified directly by silica gel column chromatography (eluent was petroleum ether or mixed petroleum ether/ethyl acetate solvent) to afford the target product, 4-(phenylalkynyl)benzaldehyde (32d, Table 1, entry 11) (99 mg, 96% yield). The product was a white solid, melting point: 98-100 °C; 1H NMR (400 MHz, CDCl3) δ 9.99 (s, 1H), 7.84 (d, J = 7.8 Hz, 2H), 7.66 (d, J = 8.0 Hz, 2H), 7.56 (dd, J = 3.4, 2.9 Hz, 2H), 7.37 (s, 3H); 13C NMR ( 100 MHz, CDCl3) δ 191.6, 135.3, 132.0, 131.7, 129.6, 128.9, 128.43, 128.41, 122.4, 93.5, 88.5.
References
[1] Tetrahedron, 2014, vol. 70, # 35, p. 5980 - 5985
[2] Transition Metal Chemistry, 2017, vol. 42, # 7, p. 579 - 585
[3] Catalysis Science and Technology, 2014, vol. 4, # 5, p. 1276 - 1285
4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE manufacturers
- Product
- 4-(2-PHENYLETH-1-YNYL)BENZALDEHYDE 57341-98-7
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-09