ChemicalBook > CAS DataBase List > BUTTPARK 83\09-70

BUTTPARK 83\09-70

Product Name: BUTTPARK 83\09-70
CAS No.: 16154-62-4
Chemical Name: BUTTPARK 83\09-70
Synonyms: BUTTPARK 83\09-70;1-(2-Chloro-4-nitrophenyl);1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPER;1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPERAZINE;Piperazine, 1-(2-chloro-4-nitrophenyl)-4-methyl-;1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine,97%
CBNumber: CB5140622
Molecular Formula: C11H14ClN3O2
Formula Weight: 255.7
MOL File: Mol file

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BUTTPARK 83\09-70 Property

Melting point:: 106 °C
Boiling point:: 384.9±42.0 °C(Predicted)
Density: 1.300±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: Solid
pka: 7.18±0.42(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FC143774
Product name: 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging: 500mg
Price: $105
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC143774
Product name: 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging: 250mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: W3507
Product name: 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging: 1g
Price: $72
Updated: 2021/12/16

Oakwood

Product number: 092578
Product name: 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Purity: 95+%
Packaging: 5g
Price: $95
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC143774
Product name: 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging: 1g
Price: $180
Updated: 2021/12/16

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BUTTPARK 83\09-70 Chemical Properties,Usage,Production

Synthesis

109-01-3

350-30-1

16154-62-4

Preparative Example 1 Synthesis of 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine: in a dry reaction flask, 3-chloro-4-fluoronitrobenzene (10.05 g, 57.2 mmol) was mixed with N-methylpiperazine (17.2 g, 172 mmol). Exothermic phenomenon was observed during the reaction and after 1 h of continuous stirring, the reaction mixture was quenched by adding water to the reaction mixture. The resulting brown solid precipitate was collected by filtration and washed with plenty of water to remove unreacted raw materials and by-products. Finally, the product was dried in air to afford 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine (14.1 g, 96% yield). The product was confirmed by 1H NMR (400 MHz, DMSO-d6) and mass spectrometry (MS) characterization: 1H NMR δ 2.24 (s, 3H), 2.43-2.55 (m, 4H), 3.11-3.24 (m, 4H), 7.28 (d, J = 9.03 Hz, 1H), 8.14 (dd, J = 9.03,2.76 Hz, 1H) , 8.21 (d, J = 2.51Hz, 1H); MS m/z 255 (M+).

References

[1] Patent: WO2011/120026, 2011, A1. Location in patent: Page/Page column 34-35
[2] Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997, vol. 36, # 4, p. 347 - 348
[3] Patent: WO2016/22460, 2016, A1. Location in patent: Page/Page column 137
[4] Patent: WO2017/66428, 2017, A1. Location in patent: Page/Page column 249

BUTTPARK 83\09-70 Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from BUTTPARK 83\09-70 manufacturers

Career Henan Chemical Co

Product: BUTTPARK 83\09-70 16154-62-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-08

16154-62-4, BUTTPARK 83\09-70Related Search:

BUTTPARK 83\09-70

1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPERAZINE

1-(2-Chloro-4-nitrophenyl)

1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPER

Piperazine, 1-(2-chloro-4-nitrophenyl)-4-methyl-

1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine,97%

16154-62-4