3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL

Product Name: 3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL
CAS No.: 123987-13-3
Chemical Name: 3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL
Synonyms: (3-(4-Methylpiperazin-1-yl);3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL;Benzenemethanol, 3-(4-methyl-1-piperazinyl)-;(3-(4-Methylpiperazin-1-yl)phenyl)methanol 95+%
CBNumber: CB51449889
Molecular Formula: C12H18N2O
Formula Weight: 206.28
MOL File: 123987-13-3.mol

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3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL Property

Boiling point:: 364.7±42.0 °C(Predicted)
Density: 1.105±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.59±0.10(Predicted)

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M331603
Product name: (3-(4-Methylpiperazin-1-yl)phenyl)methanol
Packaging: 500mg
Price: $175
Updated: 2021/12/16

Apolloscientific

Product number: OR301206
Product name: (3-(4-Methylpiperazin-1-yl)phenyl)methanol
Purity: 95+%
Packaging: 1g
Price: $124
Updated: 2021/12/16

AK Scientific

Product number: X9576
Product name: (3-(4-Methylpiperazin-1-yl)phenyl)methanol
Packaging: 1g
Price: $172
Updated: 2021/12/16

Matrix Scientific

Product number: 073774
Product name: (3-(4-Methylpiperazin-1-yl)phenyl)methanol
Purity: 95+%
Packaging: 250mg
Price: $416
Updated: 2021/12/16

AK Scientific

Product number: X9576
Product name: (3-(4-Methylpiperazin-1-yl)phenyl)methanol
Packaging: 5g
Price: $442
Updated: 2021/12/16

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3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL Chemical Properties,Usage,Production

Synthesis

109-01-3

15852-73-0

123987-13-3

GENERAL STEPS: To a solution of 3-bromobenzyl alcohol (570 mg, 3.05 mmol) in tetrahydrofuran (THF, 5 mL) was added lithium hexamethyldisilanilide (LHMDS, 7.43 mL, 7.43 mmol) and the reaction mixture was stirred for 30 min at room temperature. Ru-phos precatalyst (97 mg, 0.133 mmol), dicyclohexyl (2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine (61.9 mg, 0.133 mmol) and N-methylpiperazine (0.441 mL, 3.98 mmol) were subsequently added. The reaction system was degassed with a stream of nitrogen and then heated to 75 °C for 1 hour. After completion of the reaction, the reaction mixture was diluted with dichloromethane (DCM) and washed with water. The organic layer was concentrated under reduced pressure and purified by silica gel column chromatography (eluent: 0-20% methanol/DCM) to afford the target product (3-(4-methylpiperazin-1-yl)benzyl alcohol (506 mg, 80% yield). Mass spectrum (electrospray positive ionization mode, ES+): theoretical molecular weight of C12H18N2O 206, measured value 207 [M+H]+.

References

[1] Patent: WO2014/31928, 2014, A2. Location in patent: Paragraph 0472

3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL Suppliers

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3-(4-METHYLPIPERAZIN-1-YL)PHENYL]METHANOL

(3-(4-Methylpiperazin-1-yl)

(3-(4-Methylpiperazin-1-yl)phenyl)methanol 95+%

Benzenemethanol, 3-(4-methyl-1-piperazinyl)-

123987-13-3