3-chloro-5-nitro-aniline

Product Name: 3-chloro-5-nitro-aniline
CAS No.: 5344-44-5
Chemical Name: 3-chloro-5-nitro-aniline
Synonyms: 3-chloro-5-nitro-aniline;3-Chloro-5-nitroaniline 98%;Benzenamine, 3-chloro-5-nitro-
CBNumber: CB51459695
Molecular Formula: C6H5ClN2O2
Formula Weight: 172.57
MOL File: 5344-44-5.mol

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3-chloro-5-nitro-aniline Property

Boiling point:: 332.7±22.0 °C(Predicted)
Density: 1.494±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 1.22±0.10(Predicted)
Appearance: Yellow to orange Solid

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C596988
Product name: 3-Chloro-5-nitroaniline
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Oakwood

Product number: 234249
Product name: 3-Chloro-5-nitroaniline
Purity: 95%
Packaging: 1g
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC140097
Product name: 3-Chloro-5-nitroaniline
Packaging: 250mg
Price: $65
Updated: 2021/12/16

Oakwood

Product number: 234249
Product name: 3-Chloro-5-nitroaniline
Purity: 95%
Packaging: 250mg
Price: $30
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4655-5-44
Product name: 3-Chloro-5-nitroaniline
Packaging: 1g
Price: $88
Updated: 2021/12/16

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3-chloro-5-nitro-aniline Chemical Properties,Usage,Production

Synthesis

618-86-0

5344-44-5

General procedure for the synthesis of 3-chloro-5-nitroaniline from 1-chloro-3,5-dinitrobenzene: 1-chloro-3,5-dinitrobenzene (0.50 g, 2.47 mmol) was dissolved in a mixed solvent of 6 mL of ethanol and 3 mL of 20% aqueous ammonium sulphide, and the reaction was carried out at reflux for 1 hour. After completion of the reaction, diluted by adding appropriate amount of water, filtered to collect the solid product and dried. The product was purified by rapid chromatography on silica gel column using 10% acetone-petroleum ether mixed solvent as eluent, and finally 3-chloro-5-nitroaniline (0.36 g, 84% yield) was obtained as an orange powder.

References

[1] Patent: US6353013, 2002, B1. Location in patent: Page column 28
[2] Patent: US2011/130415, 2011, A1. Location in patent: Page/Page column 65
[3] Patent: WO2015/25197, 2015, A1. Location in patent: Paragraph 00070
[4] Journal of the Chemical Society, 1905, vol. 87, p. 1265
[5] Bulletin de la Societe Chimique de France, 1938, vol. <5> 5, p. 1441,1444

3-chloro-5-nitro-aniline Preparation Products And Raw materials

Raw materials

Preparation Products

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3-chloro-5-nitro-aniline Suppliers

China 36 India 1 United Kingdom 2 United States 4 Global 43

Energy Chemical

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Hangzhou Molcore Biopharmatech Co.,Ltd

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View Lastest Price from 3-chloro-5-nitro-aniline manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 3-chloro-5-nitro-aniline 5344-44-5
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-17

5344-44-5, 3-chloro-5-nitro-anilineRelated Search:

3-chloro-5-nitro-aniline

3-Chloro-5-nitroaniline 98%

Benzenamine, 3-chloro-5-nitro-

5344-44-5