3-Methylpicolinamide

Product Name: 3-Methylpicolinamide
CAS No.: 937648-82-3
Chemical Name: 3-Methylpicolinamide
Synonyms: 3-Methylpicolinamide;3-Methyl-2-pyridinecarboxamide;2-Pyridinecarboxamide,3-methyl-;3-Methylpicolinamide ISO 9001：2015 REACH
CBNumber: CB51465599
Molecular Formula: C7H8N2O
Formula Weight: 136.15
MOL File: 937648-82-3.mol

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3-Methylpicolinamide Property

Boiling point:: 291 ºC
Density: 1.157
Flash point:: 130 ºC
storage temp.: Sealed in dry,Room Temperature
pka: 15.09±0.50(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M321475
Product name: 3-Methylpicolinamide
Packaging: 100mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-1-8J
Product name: 3-Methylpyridine-2-carboxamide
Packaging: 1g
Price: $216
Updated: 2021/12/16

Matrix Scientific

Product number: 085039
Product name: 3-Methylpyridine-2-carboxamide
Purity: 97%
Packaging: 1g
Price: $341
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0068244
Product name: 3-METHYLPYRIDINE-2-CARBOXAMIDE
Purity: 95.00%
Packaging: 1G
Price: $785.86
Updated: 2021/12/16

Atlantic Research Chemicals

Product number: XS002150
Product name: 3-Methylpyridine-2-carboxamide
Purity: 95%
Packaging: 250mgs:
Price: $60.09
Updated: 2021/12/16

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3-Methylpicolinamide Chemical Properties,Usage,Production

Synthesis

20970-75-6

937648-82-3

General procedure for the synthesis of 3-methyl-2-pyridinecarboxamide from 2-cyano-3-methylpyridine: 2-cyano-3-methylpyridine (2.36 g, 20 mmol) was mixed with concentrated sulfuric acid (12.5 mL), and stirred for 25 min at 80 °C. Upon completion of the reaction, the solution was cooled to room temperature and slowly poured into water (80 mL), which was subsequently neutralized by the addition of saturated aqueous sodium carbonate solution. The reaction mixture was extracted with dichloromethane (3 x 80 mL), the organic layers were combined and dried with anhydrous magnesium sulfate. The organic layer was concentrated under reduced pressure to afford 3-methyl-2-pyridinecarboxamide as a white solid (2.65 g, 97% yield). The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 8.43 (dd, 1H), 7.93 (brs, 1H), 7.62 (dd, 1H), 7.35 (dd, 1H), 5.44 (brs, 1H), 2.76 (s, 3H).

References

[1] Patent: WO2013/119639, 2013, A1. Location in patent: Page/Page column 74; 75
[2] Applied Organometallic Chemistry, 2012, vol. 26, # 7, p. 377 - 382
[3] Synthetic Communications, 2014, vol. 44, # 4, p. 474 - 480

3-Methylpicolinamide Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Methylpicolinamide Suppliers

China 25 Germany 1 India 2 Ukraine 1 United Kingdom 1 United States 10 Global 40

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
Fax: 86-021-50426522,50426273
Email: sales@jingyan-chemical.com
Country: China
ProdList: 9976
Advantage: 60

Zhengzhou Guancheng Laboratory equipment Sales

Tel: 0371-88888888 272369594
Fax: QQ:272369594
Email: 2723695949@qq.com
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ProdList: 4959
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Chengdu Research Accelerators Technology Co., Ltd.

Tel: 028-64353063
Fax: 028-64353063 QQ:784253935
Email: reacchemical@163.com
Country: China
ProdList: 5253
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Aikon International Limited

Tel: 025-66113011 13155353615
Fax: (7)02557626880
Email: qzhang@aikonchem.com
Country: China
ProdList: 15394
Advantage: 58

ANHUI WITOP BIOTECH CO., LTD

Tel: +8615255079626
Email: eric@witopchemical.com
Country: China
ProdList: 23541
Advantage: 58

Dideu Industries Group Limited

Tel: +86-29-89586680 +86-15129568250
Email: 1026@dideu.com
Country: China
ProdList: 20284
Advantage: 58

Career Henan Chemica Co

Tel: +86-0371-86658258 +8613203830695
Fax: 0371-86658258
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Country: China
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Henan Lien Chemical Products Co., Ltd.

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Email: 535046669@qq.com
Country: China
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Hubei xin bonus chemical co. LTD

Tel: 86-13657291602
Fax: 027-59338440
Email: linda@hubeijusheng.com
Country: CHINA
ProdList: 22963
Advantage: 58

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View Lastest Price from 3-Methylpicolinamide manufacturers

Dideu Industries Group Limited

Product: 3-Methylpicolinamide 937648-82-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-30

937648-82-3, 3-MethylpicolinamideRelated Search:

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3-Methylpicolinamide

2-Pyridinecarboxamide,3-methyl-

3-Methyl-2-pyridinecarboxamide

3-Methylpicolinamide ISO 9001：2015 REACH

937648-82-3