3-Methylpicolinamide

Product Name: 3-Methylpicolinamide
CAS No.: 937648-82-3
Chemical Name: 3-Methylpicolinamide
Synonyms: 3-Methylpicolinamide;3-Methyl-2-pyridinecarboxamide;2-Pyridinecarboxamide,3-methyl-;3-Methylpicolinamide ISO 9001：2015 REACH
CBNumber: CB51465599
Molecular Formula: C7H8N2O
Formula Weight: 136.15
MOL File: 937648-82-3.mol

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3-Methylpicolinamide Property

Boiling point:: 291 ºC
Density: 1.157
Flash point:: 130 ºC
storage temp.: Sealed in dry,Room Temperature
pka: 15.09±0.50(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M321475
Product name: 3-Methylpicolinamide
Packaging: 100mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-1-8J
Product name: 3-Methylpyridine-2-carboxamide
Packaging: 1g
Price: $216
Updated: 2021/12/16

Matrix Scientific

Product number: 085039
Product name: 3-Methylpyridine-2-carboxamide
Purity: 97%
Packaging: 1g
Price: $341
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0068244
Product name: 3-METHYLPYRIDINE-2-CARBOXAMIDE
Purity: 95.00%
Packaging: 1G
Price: $785.86
Updated: 2021/12/16

Atlantic Research Chemicals

Product number: XS002150
Product name: 3-Methylpyridine-2-carboxamide
Purity: 95%
Packaging: 250mgs:
Price: $60.09
Updated: 2021/12/16

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3-Methylpicolinamide Chemical Properties,Usage,Production

Synthesis

20970-75-6

937648-82-3

General procedure for the synthesis of 3-methyl-2-pyridinecarboxamide from 2-cyano-3-methylpyridine: 2-cyano-3-methylpyridine (2.36 g, 20 mmol) was mixed with concentrated sulfuric acid (12.5 mL), and stirred for 25 min at 80 °C. Upon completion of the reaction, the solution was cooled to room temperature and slowly poured into water (80 mL), which was subsequently neutralized by the addition of saturated aqueous sodium carbonate solution. The reaction mixture was extracted with dichloromethane (3 x 80 mL), the organic layers were combined and dried with anhydrous magnesium sulfate. The organic layer was concentrated under reduced pressure to afford 3-methyl-2-pyridinecarboxamide as a white solid (2.65 g, 97% yield). The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 8.43 (dd, 1H), 7.93 (brs, 1H), 7.62 (dd, 1H), 7.35 (dd, 1H), 5.44 (brs, 1H), 2.76 (s, 3H).

References

[1] Patent: WO2013/119639, 2013, A1. Location in patent: Page/Page column 74; 75
[2] Applied Organometallic Chemistry, 2012, vol. 26, # 7, p. 377 - 382
[3] Synthetic Communications, 2014, vol. 44, # 4, p. 474 - 480

3-Methylpicolinamide Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Methylpicolinamide Suppliers

China 25 Germany 1 India 2 Ukraine 1 United Kingdom 1 United States 10 Global 40

Alchem Pharmtech,Inc.

Tel: 8485655694
Email: sales@alchempharmtech.com
Country: United States
ProdList: 63687
Advantage: 58

Advanced Chemical Intermediates Ltd.

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ProdList: 4893
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SynQuest Laboratories, Inc.

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ProdList: 6871
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Matrix Scientific

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Advantage: 80

Alfa Chemistry

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ProdList: 6814
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Sphinx Scientific Laboratory, LLC

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ProdList: 3343
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American Custom Chemicals Corporation

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Country: United States
ProdList: 6820
Advantage: 51

Ryan Scientific, Inc.

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ProdList: 6439
Advantage: 60

AstaTech, Inc

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ProdList: 6371
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Accel Pharmtech, LLC

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Email: info@accelpharmtech.com
Country: United States
ProdList: 361
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View Lastest Price from 3-Methylpicolinamide manufacturers

Dideu Industries Group Limited

Product: 3-Methylpicolinamide 937648-82-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-30

937648-82-3, 3-MethylpicolinamideRelated Search:

PYRIDINE-2,3-DICARBOXAMIDE CHEMBRDG-BB 6081020 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione 2,3-Pyridinedicarboximide, N-(5,5-dimethyl-2-oxotetrahydro-3-furyl)- 2-(AMINOCARBONYL)NICOTINIC ACID

3-Methylpicolinamide

2-Pyridinecarboxamide,3-methyl-

3-Methyl-2-pyridinecarboxamide

3-Methylpicolinamide ISO 9001：2015 REACH

937648-82-3