H-ACH-OME
- Product Name
- H-ACH-OME
- CAS No.
- 37993-32-1
- Chemical Name
- H-ACH-OME
- Synonyms
- H-ACH-OME;Methyl 1-Aminocyclohexanecarboxylate HCl;methyl 1-aminocyclohexane-1-carboxylate hydrochloride;Methyl 1-aminocyclohexanecarboxylate HYDROCHLORIDE Salt;1-Aminocyclohexanecarboxylic acid methyl ester hydrochloride;1-Amino-1-cyclohexanecarboxylic acid methyl ester hydrochloride
- CBNumber
- CB51474373
- Molecular Formula
- C8H16ClNO2
- Formula Weight
- 193.67114
- MOL File
- 37993-32-1.mol
H-ACH-OME Property
- Melting point:
- 210-212 °C(Solv: methanol (67-56-1); ethyl ether (60-29-7))
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M331713
- Product name
- Methyl1-aminocyclohexanecarboxylatehydrochloride
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 4874AB
- Product name
- Methyl1-aminocyclohexanecarboxylatehydrochloride
- Packaging
- 1g
- Price
- $76
- Updated
- 2021/12/16
- Product number
- 174583
- Product name
- Methyl 1-aminocyclohexanecarboxylate hydrochloride
- Packaging
- 1g
- Price
- $432
- Updated
- 2021/12/16
- Product number
- CHM0122269
- Product name
- METHYL 1-AMINOCYCLOHEXANECARBOXYLATE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $852.55
- Updated
- 2021/12/16
- Product number
- 174583
- Product name
- Methyl 1-aminocyclohexanecarboxylate hydrochloride
- Packaging
- 5g
- Price
- $1206
- Updated
- 2021/12/16
H-ACH-OME Chemical Properties,Usage,Production
Synthesis
67-56-1
2756-85-6
37993-32-1
3.3 Synthesis of methyl 1-aminocyclohexanecarboxylate hydrochloride To a 20 mL methanol suspension containing 2 g (14 mmol) of 1-aminocyclohexanecarboxylic acid, hydrogen chloride gas was passed for 2 min. Subsequently, 1.2 mL (16.8 mmol) of thionyl chloride was slowly added to the resulting solution and the reaction mixture was heated to reflux for 6 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure to remove the solvent. The concentrated residue was dissolved in 5 mL of methanol, and then 50 mL of ether was slowly added to this solution to induce precipitation of the product. Ultimately, 2.3 g of methyl 1-aminocyclohexanecarboxylate hydrochloride in white powder form was obtained in 85% yield.
References
[1] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006, vol. 45, # 8, p. 1942 - 1944
[2] Patent: US2011/9426, 2011, A1. Location in patent: Page/Page column 13
[3] Patent: WO2013/19091, 2013, A2. Location in patent: Paragraph 881-883
[4] Patent: US2014/206875, 2014, A1. Location in patent: Paragraph 0482-0484
[5] Journal of Medicinal Chemistry, 1984, vol. 27, # 12, p. 1663 - 1668
H-ACH-OME Preparation Products And Raw materials
Raw materials
Preparation Products
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