ChemicalBook > CAS DataBase List > (3-BROMO-PHENOXY)-ACETIC ACID

(3-BROMO-PHENOXY)-ACETIC ACID

Product Name
(3-BROMO-PHENOXY)-ACETIC ACID
CAS No.
1798-99-8
Chemical Name
(3-BROMO-PHENOXY)-ACETIC ACID
Synonyms
2-(3-BroMophenoxy)acetic acid;2-(3-bromophenoxy)ethanoic acid;Acetic acid, 2-(3-bromophenoxy)-;(3-bromophenoxy)acetic acid(SALTDATA: FREE)
CBNumber
CB51491156
Molecular Formula
C8H7BrO3
Formula Weight
231.04
MOL File
1798-99-8.mol
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(3-BROMO-PHENOXY)-ACETIC ACID Property

storage temp. 
Sealed in dry,Room Temperature
pka
pK1: 3.09 (25°C)
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B687228
Product name
3-Bromophenoxyaceticacid
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
B687228
Product name
3-Bromophenoxyaceticacid
Packaging
500mg
Price
$65
Updated
2021/12/16
Matrix Scientific
Product number
028299
Product name
(3-Bromophenoxy)acetic acid
Packaging
500mg
Price
$45
Updated
2021/12/16
Matrix Scientific
Product number
028299
Product name
(3-Bromophenoxy)acetic acid
Packaging
1g
Price
$69
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB112805
Product name
(3-Bromophenoxy)acetic acid
Packaging
500mg
Price
$75
Updated
2021/12/16
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(3-BROMO-PHENOXY)-ACETIC ACID Chemical Properties,Usage,Production

Synthesis

111758-64-6

1798-99-8

The general procedure for the synthesis of 2-(3-bromophenoxy)acetic acid from methyl 2-(3-bromophenoxy)acetate was as follows: lithium hydroxide monohydrate (8.41 g, 0.2 mol) was slowly added to 100 ml of a water-THF solvent mixture (3:1, v/v) of methyl 2-(3-bromophenoxy)acetate (19.66 g, 80 mmol) at 0 °C. The reaction temperature was maintained at 0 °C and stirring was continued for 15 min. Upon completion of the reaction, the reaction mixture was acidified with aqueous 3N hydrochloric acid to pH < 3. Subsequently, extraction was carried out with ether and the organic phases were combined and dried with anhydrous magnesium sulfate. After filtration to remove the desiccant, the solvent was evaporated under reduced pressure to give 18.21 g of the white solid product 2-(3-bromophenoxy)acetic acid in 98% yield. The melting point of the product was 108 °C. The NMR hydrogen spectrum (200 MHz, CDCl3) data were as follows: δ 4.70 (s, 2H, CH2-O), 6.80-6.90 (m, 1H, ArH), 7.05-7.10 (m, 1H, ArH), 7.15-7.20 (m, 2H, ArH), 9.40-9.05 (br s, 1H, COOH).

References

[1] Patent: US6239284, 2001, B1

(3-BROMO-PHENOXY)-ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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1798-99-8, (3-BROMO-PHENOXY)-ACETIC ACIDRelated Search:

3,5-DIBROMO-4-HYDROXYPHENOXYACETIC ACID (3-BROMO-PHENOXY)-ACETIC ACID 2-(3-BROMOPHENOXY)PROPANOIC ACID AKOS B005230 (5-BROMO-4-FORMYL-2-METHOXYPHENOXY)ACETIC ACID AKOS B005135 AKOS B005141 AKOS B005144 AKOS B005143 AKOS B005142 methyl 2-(3-bromophenoxy)acetate AKOS B005232 AKOS B005138 AKOS B005136 AKOS B005137 AKOS B005134 (5-BROMO-2-ETHOXY-4-FORMYLPHENOXY)ACETIC ACID AKOS B005139

  • (3-bromophenoxy)acetic acid(SALTDATA: FREE)
  • 2-(3-BroMophenoxy)acetic acid
  • 2-(3-bromophenoxy)ethanoic acid
  • Acetic acid, 2-(3-bromophenoxy)-
  • 1798-99-8