4-TETRAZOL-1-YL-PHENOL
- Product Name
- 4-TETRAZOL-1-YL-PHENOL
- CAS No.
- 64001-11-2
- Chemical Name
- 4-TETRAZOL-1-YL-PHENOL
- Synonyms
- 4-(1H-Tetrazol-1-yl);Phenol, 4-(1-tetrazolyl)-;Phenol, 4-(1H-tetrazol-1-yl)-;4-Tetrazol-1-yl-phenol, 97%min;4-(1H-1,2,3,4-tetrazol-1-yl)phenol;4-(1H-tetrazol-1-yl)phenol(SALTDATA: FREE)
- CBNumber
- CB51491787
- Molecular Formula
- C7H6N4O
- Formula Weight
- 162.15
- MOL File
- 64001-11-2.mol
4-TETRAZOL-1-YL-PHENOL Property
- Boiling point:
- 370.2±44.0 °C(Predicted)
- Density
- 1.46±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 8.68±0.13(Predicted)
- Appearance
- white solid
Safety
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H228Flammable solid
H341Suspected of causing genetic defects
- Precautionary statements
-
P201Obtain special instructions before use.
P202Do not handle until all safety precautions have been read and understood.
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P240Ground/bond container and receiving equipment.
P241Use explosion-proof electrical/ventilating/lighting/…/equipment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P281Use personal protective equipment as required.
P308+P313IF exposed or concerned: Get medical advice/attention.
P370+P378In case of fire: Use … for extinction.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- X7159
- Product name
- 4-Tetrazol-1-yl-phenol
- Packaging
- 1g
- Price
- $151
- Updated
- 2021/12/16
- Product number
- 057718
- Product name
- 4-Tetrazol-1-yl-phenol
- Purity
- 95%
- Packaging
- 1g
- Price
- $174
- Updated
- 2021/12/16
- Product number
- 057718
- Product name
- 4-Tetrazol-1-yl-phenol
- Purity
- 95%
- Packaging
- 5g
- Price
- $478
- Updated
- 2021/12/16
- Product number
- A237175
- Product name
- 4-(1H-Tetrazol-1-yl)phenol
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $7
- Updated
- 2021/12/16
- Product number
- A237175
- Product name
- 4-(1H-Tetrazol-1-yl)phenol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $9
- Updated
- 2021/12/16
4-TETRAZOL-1-YL-PHENOL Chemical Properties,Usage,Production
Synthesis
123-30-8
122-51-0
64001-11-2
GENERAL METHODS: Fe3O4WO3-EAE-SO3H(III) (0.01 g) was added to a solution in water (5 mL) containing 4-aminophenol (0.093 g, 1.0 mmol), triethyl orthoformate (0.177 g, 1.2 mmol) and 1-butyl-3-methylimidazolium azide (0.216 g, 1.2 mmol). The reaction mixture was magnetically stirred at 60 °C for 30 min. Upon completion of the reaction (monitored by TLC), the mixture was cooled to room temperature and the catalyst was separated with an external magnet. The resulting solution was extracted with EtOAc (3 x 15 mL). The organic layers were combined, washed with brine, dried over anhydrous Na2SO4 and concentrated under reduced pressure. The crude product was recrystallized with ethyl acetate/hexane (1/9 v/v) to give pure 4-tetrazol-1-ylphenol (1.48 g, 95% yield). The recovered catalyst was washed with hot ethyl acetate and dried at 60 °C for 2 h for subsequent recycling.
References
[1] Journal of the Iranian Chemical Society, 2014, vol. 11, # 1, p. 91 - 99
[2] Bulletin of the Chemical Society of Japan, 2017, vol. 90, # 10, p. 1119 - 1128
[3] Patent: US2012/53180, 2012, A1. Location in patent: Page/Page column 13
4-TETRAZOL-1-YL-PHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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