ChemicalBook > CAS DataBase List > 2-CHLORO-5-NITRONICOTINAMIDE

2-CHLORO-5-NITRONICOTINAMIDE

Product Name
2-CHLORO-5-NITRONICOTINAMIDE
CAS No.
60524-15-4
Chemical Name
2-CHLORO-5-NITRONICOTINAMIDE
Synonyms
Nicotinamide Impurity 75;2-CHLORO-5-NITRONICOTINAMIDE;2-Chloro-5-nitro-3-Pyridinecarboxamide;2-Chloro-5-nitro-3-pyridinecarboxylamide;3-Pyridinecarboxamide, 2-chloro-5-nitro-
CBNumber
CB51493857
Molecular Formula
C6H4ClN3O3
Formula Weight
201.57
MOL File
60524-15-4.mol
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2-CHLORO-5-NITRONICOTINAMIDE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C612060
Product name
2-Chloro-5-nitronicotinamide
Packaging
100mg
Price
$90
Updated
2021/12/16
TRC
Product number
C612060
Product name
2-Chloro-5-nitronicotinamide
Packaging
500mg
Price
$350
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0058122
Product name
2-CHLORO-5-NITRONICOTINAMIDE
Purity
95.00%
Packaging
1G
Price
$437.85
Updated
2021/12/16
Matrix Scientific
Product number
096574
Product name
2-Chloro-5-nitronicotinamide
Purity
95+%
Packaging
5g
Price
$655
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0058122
Product name
2-CHLORO-5-NITRONICOTINAMIDE
Purity
95.00%
Packaging
2.5G
Price
$1227.82
Updated
2021/12/16
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2-CHLORO-5-NITRONICOTINAMIDE Chemical Properties,Usage,Production

Synthesis Reference(s)

Journal of Medicinal Chemistry, 20, p. 129, 1977 DOI: 10.1021/jm00211a027

Synthesis

135795-55-0

60524-15-4

Compound 21 (8.3 g, 0.04 mol) was added to thionyl chloride (80 mL) and heated to reflux for 3 hours. Upon completion of the reaction, excess thionyl chloride was removed by distillation under reduced pressure. Acetone (240 mL) was added to the residue with stirring at 25 °C and ammonia was added slowly and dropwise, the reaction lasted for 10 min. The reaction mixture was concentrated to one-fourth of the original volume and the concentrate was poured into 200 g of crushed ice, precipitating a yellow solid. The solid was collected by filtration to give 4.5 g of the target product 2-chloro-5-nitro-3-pyridine carboxamide in 54.2% yield. The melting point of the product was 177.3-178.2 °C.

References

[1] Russian Chemical Bulletin, 2005, vol. 54, # 8, p. 1907 - 1914
[2] Patent: EP2366691, 2011, A1. Location in patent: Page/Page column 10
[3] Antimicrobial Agents and Chemotherapy, 2014, vol. 58, # 1, p. 55 - 60

2-CHLORO-5-NITRONICOTINAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-5-NITRONICOTINAMIDE Suppliers

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60524-15-4, 2-CHLORO-5-NITRONICOTINAMIDERelated Search:


  • 2-CHLORO-5-NITRONICOTINAMIDE
  • 2-Chloro-5-nitro-3-Pyridinecarboxamide
  • 3-Pyridinecarboxamide, 2-chloro-5-nitro-
  • 2-Chloro-5-nitro-3-pyridinecarboxylamide
  • Nicotinamide Impurity 75
  • 60524-15-4