ChemicalBook > CAS DataBase List > 3-(BENZYLOXY)PROPAN-1-AMINE

3-(BENZYLOXY)PROPAN-1-AMINE

Product Name: 3-(BENZYLOXY)PROPAN-1-AMINE
CAS No.: 16728-64-6
Chemical Name: 3-(BENZYLOXY)PROPAN-1-AMINE
Synonyms: 3-benzyloxy-propylaMine;3-Benzyloxypropane-1-amine;3-(BENZYLOXY)PROPAN-1-AMINE;3-(benzyloxy)-1-propanamine;1-Amino-3-(benzyloxy)propane;3-phenylmethoxypropan-1-amine;3-(BENZYLOXY)PROPAN-1-AMINE 97%;4-Benzofuranpropanenitrile,β-oxo-;1-Propanamine, 3-(phenylmethoxy)-;[3-(benzyloxy)propyl]amine hydrochloride
CBNumber: CB51497042
Molecular Formula: C10H15NO
Formula Weight: 165.23
MOL File: 16728-64-6.mol

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3-(BENZYLOXY)PROPAN-1-AMINE Property

Boiling point:: 103 °C(Press: 2 Torr)
Density: 0.999±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 9.74±0.10(Predicted)

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Safety

HS Code: 2922190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H319Causes serious eye irritation
Precautionary statements: P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B521803
Product name: 3-(Benzyloxy)propan-1-amine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB133069
Product name: [3-(Benzyloxy)propyl]amine hydrochloride
Packaging: 250mg
Price: $57.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB133069
Product name: [3-(Benzyloxy)propyl]amine hydrochloride
Packaging: 500mg
Price: $100
Updated: 2021/12/16

Matrix Scientific

Product number: 114186
Product name: 3-(Benzyloxy)propan-1-amine
Purity: 97%
Packaging: 500mg
Price: $129
Updated: 2021/12/16

AK Scientific

Product number: 8527AA
Product name: 3-(Benzyloxy)propan-1-amine
Packaging: 250mg
Price: $154
Updated: 2021/12/16

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3-(BENZYLOXY)PROPAN-1-AMINE Chemical Properties,Usage,Production

Synthesis Reference(s)

Synthesis, p. 590, 1975 DOI: 10.1055/s-1975-23843

Synthesis

100-39-0

156-87-6

16728-64-6

A 60% sodium hydride dispersion (4 g, 0.1 mol) was slowly added to a stirred solution of 3-amino-1-propanol (7.51 g, 0.1 mol) in tetrahydrofuran (THF, 150 mL) at room temperature. The reaction mixture was stirred under nitrogen protection for 30 min before benzyl bromide (11.9 mL, 0.1 mol) was added. The reaction was continued to be stirred at room temperature for 10 hours, followed by vacuum concentration. The concentrated residue was partitioned between a 1N aqueous hydrochloric acid solution and dichloromethane (CH2Cl2). The aqueous layer was adjusted to pH 10 with 10% aqueous sodium hydroxide and subsequently extracted with dichloromethane (3 x 100 mL). The organic phases were combined, dried with magnesium sulfate (MgSO4) and concentrated in vacuum. The residue was purified by silica gel column chromatography using dichloromethane/methanol (3:1 to 2:1, v/v) as eluent to give 3-(benzyloxy)propylamine (8.3% yield) as a yellow oil. A solution of 1,3-dicyclohexylcarbodiimide (14.4 mg, 0.07 mmol) in dichloromethane (2 mL) was added dropwise to a solution of compound 5 (32 mg, 0.07 mmol), 3-(benzyloxy)propylamine (0.07 mmol), and 1-hydroxybenzotriazole hydrate (9.5 mg, 0.07 mmol) in dichloromethane (5 mL) at 0°C . The reaction mixture was stirred at room temperature for 18 h and then concentrated under vacuum. The residue was purified by silica gel column chromatography using dichloromethane/methanol (30:1, v/v) as eluent to afford compound 8 (36 mg, 85% yield) as a light yellow liquid.1H NMR (CDCl3) δ 8.05 (s, 1H, H4), 7.44 (d, 1H, H5, J = 8.7Hz), 7.19-7.28 (m, 11H H6 + 2 × OCH2Ph), 6.78-6.82 (m, 3H, H2' + H5' + H6'), 6.06 (AB, 2H, 3',4'-OCH2O-, J = 6.9 Hz, J = 1.5 Hz), 5.84 (AB, 2H, 7,8-OCH2O-, J = 4.2 Hz, J = 1.5 Hz), 4.45 (s 4H, 2 × OCH2Ph), 4.38 (s, 2H, 2-CH2OBn), 3.55 (m, 4H, 3-CONHCH2CH2CH2OBn), 1.87 (quintuple peak, 2H, 3-CONHCH2CH2CH2OBn, J = 6.3 Hz); MS (FAB, positive) m/z 604 [M + H]+.

References

[1] Journal of Medicinal Chemistry, 2005, vol. 48, # 2, p. 534 - 546
[2] Patent: WO2005/107742, 2005, A1. Location in patent: Page/Page column 40-41

3-(BENZYLOXY)PROPAN-1-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(BENZYLOXY)PROPAN-1-AMINE manufacturers

Career Henan Chemical Co

Product: 3-benzyloxypropylamine 16728-64-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

16728-64-6, 3-(BENZYLOXY)PROPAN-1-AMINERelated Search:

3-Benzyloxypropane-1-amine

3-benzyloxy-propylaMine

[3-(benzyloxy)propyl]amine hydrochloride

3-(benzyloxy)propan-1-amine hydrochloride

3-(benzyloxy)-1-propanamine

1-Propanamine, 3-(phenylmethoxy)-

3-phenylmethoxypropan-1-amine

4-Benzofuranpropanenitrile,β-oxo-

1-Amino-3-(benzyloxy)propane

3-(BENZYLOXY)PROPAN-1-AMINE 97%

3-(BENZYLOXY)PROPAN-1-AMINE

16728-64-6