ChemicalBook > CAS DataBase List > 4-chloro-3-iodobenzaldehyde
4-chloro-3-iodobenzaldehyde
- Product Name
- 4-chloro-3-iodobenzaldehyde
- CAS No.
- 276866-90-1
- Chemical Name
- 4-chloro-3-iodobenzaldehyde
- Synonyms
- 4-chloro-3-iodobenzaldehyde;4-dhloro-3-iodobenzaldehyde;Benzaldehyde, 4-chloro-3-iodo-
- CBNumber
- CB51559467
- Molecular Formula
- C7H4ClIO
- Formula Weight
- 266.46
- MOL File
- 276866-90-1.mol
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4-chloro-3-iodobenzaldehyde Property
- Melting point:
- 117 °C
- Boiling point:
- 304.0±27.0 °C(Predicted)
- Density
- 1.971±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- White to off-white Solid
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Safety
- HS Code
- 2913000090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Ark Pharm
- Product number
- AK177782
- Product name
- 4-Chloro-3-iodobenzaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $119
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 2615-M-06
- Product name
- 4-Chloro-3-iodobenzaldehyde
- Packaging
- 250mg
- Price
- $157
- Updated
- 2021/12/16
AK Scientific
- Product number
- 5972CS
- Product name
- 4-Chloro-3-iodobenzaldehyde
- Packaging
- 250mg
- Price
- $242
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 2615-M-06
- Product name
- 4-Chloro-3-iodobenzaldehyde
- Packaging
- 1g
- Price
- $336
- Updated
- 2021/12/16
AK Scientific
- Product number
- 5972CS
- Product name
- 4-Chloro-3-iodobenzaldehyde
- Packaging
- 5g
- Price
- $1327
- Updated
- 2021/12/16
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4-chloro-3-iodobenzaldehyde Chemical Properties,Usage,Production
Synthesis
104-88-1
276866-90-1
The general procedure for the synthesis of 3-iodo-4-chlorobenzaldehyde from 4-chlorobenzaldehyde was as follows: iodine (1.12 g, 4.4 mmol) and sodium iodate (400 mg, 2.2 mmol) were added to a reaction vessel containing sulphuric acid (30 ml), and stirred at room temperature for 30 minutes. Subsequently, 4-chlorobenzaldehyde (1.40 g, 10.0 mmol) was added to the reaction mixture and stirring was continued for 1 hour at room temperature. After completion of the reaction, the reaction mixture was poured into ice water and the resulting solid was separated by filtration. After washing the solid with water to neutral, the solid was dissolved in ethanol and recrystallized to give 1.06 g (4.00 mmol, 40% yield) of 3-iodo-4-chlorobenzaldehyde.
References
[1] Bulletin of the Chemical Society of Japan, 2000, vol. 73, # 4, p. 951 - 956
[2] Tetrahedron, 2004, vol. 60, # 41, p. 9113 - 9119
[3] Synthesis, 2006, # 7, p. 1195 - 1199
[4] Patent: KR2016/149561, 2016, A. Location in patent: Paragraph 0125; 0126; 0127
[5] European Journal of Medicinal Chemistry, 2016, vol. 123, p. 180 - 190
4-chloro-3-iodobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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