ChemicalBook > CAS DataBase List > 6-bromo-1-methyl-1H-indazol-3-amine

6-bromo-1-methyl-1H-indazol-3-amine

Product Name: 6-bromo-1-methyl-1H-indazol-3-amine
CAS No.: 1214899-85-0
Chemical Name: 6-bromo-1-methyl-1H-indazol-3-amine
Synonyms: 6-bromo-1-methylindazol-3-amine;6-bromo-1-methyl-1H-indazol-3-amine;3-Amino-6-bromo-1-methyl-1H-indazole;1H-Indazol-3-amine, 6-bromo-1-methyl-;Piperidine,1-(3-chloropropyl)-,hydrochloride(1:5)
CBNumber: CB51560139
Molecular Formula: C8H8BrN3
Formula Weight: 226.07
MOL File: 1214899-85-0.mol

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6-bromo-1-methyl-1H-indazol-3-amine Property

Boiling point:: 378.4±22.0 °C(Predicted)
Density: 1.76±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 3.12±0.50(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C8H8BrN3/c1-12-7-4-5(9)2-3-6(7)8(10)11-12/h2-4H,1H3,(H2,10,11)
InChIKey: SJCNMXPRXAGVMK-UHFFFAOYSA-N
SMILES: N1(C)C2=C(C=CC(Br)=C2)C(N)=N1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B808375
Product name: 6-Bromo-1-methyl-1H-indazol-3-amine
Packaging: 100mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B808375
Product name: 6-Bromo-1-methyl-1H-indazol-3-amine
Packaging: 250mg
Price: $100
Updated: 2021/12/16

TRC

Product number: B808375
Product name: 6-Bromo-1-methyl-1H-indazol-3-amine
Packaging: 500mg
Price: $165
Updated: 2021/12/16

Matrix Scientific

Product number: 076261
Product name: 3-Amino-6-bromo-1-methyl-1H-indazole
Purity: 95+%
Packaging: 1g
Price: $577
Updated: 2021/12/16

Matrix Scientific

Product number: 076261
Product name: 3-Amino-6-bromo-1-methyl-1H-indazole
Purity: 95+%
Packaging: 250mg
Price: $231
Updated: 2021/12/16

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6-bromo-1-methyl-1H-indazol-3-amine Chemical Properties,Usage,Production

Synthesis

404827-77-6

74-88-4

1214899-85-0

Intermediate 3. Synthesis of 6-bromo-1-methyl-1H-indazol-3-amine: 6-bromo-1H-indazol-3-amine (788 mg, 3.71 mmol) was dissolved in dimethylformamide (3 mL) and cooled to 0 °C. Sodium hydride (60% oil dispersion; 163 mg, 6.79 mmol) was added in batches under stirring. The reaction mixture was continued to be stirred at 0 °C for 30 min. Subsequently, iodomethane (225 μL, 4.09 mmol) was added dropwise to the mixture and the reaction was stirred for 2 h at room temperature. Upon completion of the reaction, water was added to the crude reaction mixture and a red solid was precipitated. The solid was collected by filtration and dried to afford the title compound in 80% yield. The product was analyzed by LRMS showing m/z: 226 (M)+, 228 (M + 2)+. 1H NMR (300 MHz, DMSO-d6) δ ppm: 3.75 (s, 3H); 5.7 (s, 2H); 7.01 (d, 1H); 7.59 (d, 1H); 7.6 (s, 1H).

References

[1] Patent: WO2016/150971, 2016, A1. Location in patent: Page/Page column 23

6-bromo-1-methyl-1H-indazol-3-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-bromo-1-methyl-1H-indazol-3-amine manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 6-bromo-1-methyl-1H-indazol-3-amine 1214899-85-0
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 10000KGS
Release date: 2025-03-02

Career Henan Chemical Co

Product: 6-bromo-1-methyl-1H-indazol-3-amine 1214899-85-0
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-02-20

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