2-Pyridin-4-ylacetohydrazide

Product Name: 2-Pyridin-4-ylacetohydrazide
CAS No.: 69583-00-2
Chemical Name: 2-Pyridin-4-ylacetohydrazide
Synonyms: 2-Pyridin-4-ylacetohydrazide;4-Pyridineacetic acid hydrazide;2-pyridin-4-ylacetohydrazide(SALTDATA: FREE)
CBNumber: CB51873837
Molecular Formula: C7H9N3O
Formula Weight: 151.17
MOL File: 69583-00-2.mol

More

Less

2-Pyridin-4-ylacetohydrazide Property

Melting point:: 85-86 °C(Solv: benzene (71-43-2))
Boiling point:: 416.8±28.0 °C(Predicted)
Density: 1.208±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 12.38±0.37(Predicted)

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: P840485
Product name: 2-(Pyridin-4-yl)acetohydrazide
Packaging: 100mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: Y5522
Product name: 2-(Pyridin-4-yl)acetohydrazide
Packaging: 10g
Price: $705
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0136600
Product name: 2-PYRIDIN-4-YLACETOHYDRAZIDE
Purity: 95.00%
Packaging: 1G
Price: $721.57
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0136600
Product name: 2-PYRIDIN-4-YLACETOHYDRAZIDE
Purity: 95.00%
Packaging: 2.5G
Price: $983.88
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0136600
Product name: 2-PYRIDIN-4-YLACETOHYDRAZIDE
Purity: 95.00%
Packaging: 5G
Price: $1168.42
Updated: 2021/12/16

More

Less

2-Pyridin-4-ylacetohydrazide Chemical Properties,Usage,Production

Synthesis

54401-85-3

69583-00-2

General procedure for the synthesis of 2-(pyridin-4-yl)acetohydrazide from ethyl 4-pyridyl acetate: a mixture of hydrazine hydrate (0.27 mL, 9.08 mmol), ethyl pyridin-4-yl acetate (0.93 mL, 6.05 mmol), and ethanol (10 mL) was heated and reacted for 10 hours at 80 °C. Subsequently, hydrazine hydrate (0.6 mL) was added to the reaction system and the reaction continued to be heated at 80 °C for 14 hours. After completion of the reaction, the reaction solution was cooled to room temperature and concentrated under vacuum. The final 2-(pyridin-4-yl)acetylhydrazine (0.86 g, 95% yield) was obtained as a white solid. The structure of the product was confirmed by 1H NMR (DMSO-d6) and mass spectra (MS): 1H NMR (DMSO-d6) δ 9.29 (s, 1H), 8.47 (d, J = 5.6 Hz, 2H), 7.27 (d, J = 5.2 Hz, 2H), 4.28 (s, 2H), 3.39 (s, 2H); MS m/z 152 (M + 1).

References

[1] European Journal of Medicinal Chemistry, 2010, vol. 45, # 11, p. 4788 - 4796
[2] Journal of Labelled Compounds and Radiopharmaceuticals, 2016, vol. 59, # 14, p. 665 - 672
[3] Patent: WO2004/101512, 2004, A2. Location in patent: Page 87
[4] ChemMedChem, 2015, vol. 10, # 11, p. 1875 - 1883
[5] Journal of the American Chemical Society, 1953, vol. 75, p. 1933,1934

2-Pyridin-4-ylacetohydrazide Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

2-Pyridin-4-ylacetohydrazide Suppliers

China 36 India 2 United Kingdom 1 United States 7 Global 46

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

ZEROSCHEM.CO.,LTD.

Tel: 10-61256048 13810278579
Fax: +86 10 61256049
Email: sales@zeroschem.com
Country: China
ProdList: 1370
Advantage: 59

Amatek Scientific Co. Ltd.

Tel: 0512-56316828 4008675858
Fax: +86-512-56316826
Email: sales@amateksci.com
Country: China
ProdList: 9874
Advantage: 55

Radiant Pharma & Tech. Co., Ltd

Tel: T:15050866711
Fax: QQ:2677337387
Email: wanglin.chen@radiant-pharma.com
Country: China
ProdList: 466
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Wuxi AppTec

Tel: 022-59987777 13552403979
Email: jia_guoqiang@wuxiapptec.com
Country: China
ProdList: 22345
Advantage: 58

Aikon International Limited

Tel: 025-66113011 13155353615
Fax: (7)02557626880
Email: qzhang@aikonchem.com
Country: China
ProdList: 15394
Advantage: 58

3A Chemicals

Tel: 400-668-9898
Fax: 010-51582189
Email: service@3achem.com
Country: China
ProdList: 20557
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

ANHUI WITOP BIOTECH CO., LTD

Tel: +8615255079626
Email: eric@witopchemical.com
Country: China
ProdList: 23541
Advantage: 58

69583-00-2, 2-Pyridin-4-ylacetohydrazideRelated Search:

Acethydrazide 2-Pyridin-4-ylacetohydrazide PYRIDINE-4-ACETAMIDE

2-Pyridin-4-ylacetohydrazide

4-Pyridineacetic acid hydrazide

2-pyridin-4-ylacetohydrazide(SALTDATA: FREE)

69583-00-2

Pyridines