2-Methylthiazole-5-carbaldehyde
- Product Name
- 2-Methylthiazole-5-carbaldehyde
- CAS No.
- 1003-60-7
- Chemical Name
- 2-Methylthiazole-5-carbaldehyde
- Synonyms
- 2-Methylthiazol-5-carbaldehyde;5-Formyl-2-methyl-1,3-thiazole;2-Methyl-5-thiazolecarbaldehyde;2-Methylthiazole-5-carbaldehyde;2-Methylthiazole-5-carboxaldehyde;2-Methyl-5-thiazolecarboxaldehyde;5-Thiazolecarboxaldehyde, 2-Methyl-;2-METHYL-1,3-THIAZOLE-5-CARBALDEHYDE;2-Methylthiazole-5-carbaldehyde≥ 99% (Assay);2-methyl-1,3-thiazole-5-carbaldehyde(SALTDATA: FREE)
- CBNumber
- CB52105766
- Molecular Formula
- C5H5NOS
- Formula Weight
- 127.16
- MOL File
- 1003-60-7.mol
2-Methylthiazole-5-carbaldehyde Property
- Boiling point:
- 110-116 °C(Press: 18 Torr)
- Density
- 1.270±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- pka
- 1.66±0.10(Predicted)
- form
- crystals
- color
- Orange
Safety
- HazardClass
- IRRITANT
- HS Code
- 2934100090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B486143
- Product name
- 2-Methylthiazole-5-carbaldehyde
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- P000126444
- Product name
- 2-Methylthiazole-5-carbaldehyde
- Purity
- 97%
- Packaging
- 250mg
- Price
- $10
- Updated
- 2021/12/16
- Product number
- P000126444
- Product name
- 2-Methylthiazole-5-carbaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $23
- Updated
- 2021/12/16
- Product number
- F10802
- Product name
- 5-Formyl-2-methylthiazole
- Purity
- 98%
- Packaging
- 1g
- Price
- $34
- Updated
- 2021/12/16
- Product number
- 027139
- Product name
- 2-Methyl-1,3-thiazole-5-carbaldehyde
- Packaging
- 500mg
- Price
- $42
- Updated
- 2021/12/16
2-Methylthiazole-5-carbaldehyde Chemical Properties,Usage,Production
Chemical Properties
Yellowish orange solid
Synthesis
2065-75-0
62-55-5
1003-60-7
Example A.1: 2-Bromomalonaldehyde (1.5 g, 9.94 mmol, 1 eq.) and thioacetamide (0.83 g, 11.05 mmol, 1.11 eq.) were suspended in dichloromethane (DCM, 10 mL) and the mixture was cooled to 0°C. Subsequently, N,N-diisopropylethylamine (DIPEA, 1.75 mL, 10.05 mmol, 1.01 eq.) was added slowly and dropwise. The resulting brown solution was stirred at room temperature for 3 days. After completion of the reaction, the organic phase was separated by diluting the reaction mixture with deionized water (50 mL). The aqueous phase was extracted three times with DCM (10 mL). The organic phases were combined, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated. The brown residue was dissolved in ether (Et2O, 20 mL) and washed twice sequentially with saturated sodium bicarbonate solution (20 mL) and saturated saline (20 mL). The organic phase was dried again with anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give pure 5-formyl-2-methylthiazole as a brown oil (0.40 g, 31% yield).
References
[1] Patent: WO2015/118019, 2015, A1. Location in patent: Page/Page column 29
[2] Journal of Medicinal Chemistry, 2000, vol. 43, # 16, p. 3168 - 3185
[3] Yakugaku Zasshi, 1953, vol. 73, p. 276
[4] Chem.Abstr., 1954, p. 2045
2-Methylthiazole-5-carbaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Methylthiazole-5-carbaldehyde manufacturers
- Product
- 2-Methylthiazole-5-carbaldehyde 1003-60-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000KG
- Release date
- 2024-07-17
- Product
- 2-Methylthiazole-5-carbaldehyde 1003-60-7
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27
- Product
- 2-Methylthiazole-5-carbaldehyde 1003-60-7
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-03