1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE

Product Name: 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE
CAS No.: 1208-75-9
Chemical Name: 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE
Synonyms: 4H-Azepin-4-one;1-benzyl-4-azepanone;1-Benzylazepan-4-one;N-Benzylazepane-4-one;hexahydro-1-(phenylMethyl)-;1-Benzylhexahydro-4-azepinone;1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE;4H-Azepin-4-one,hexahydro-1-(phenylmethyl)-
CBNumber: CB5229835
Molecular Formula: C13H17NO
Formula Weight: 203.28
MOL File: 1208-75-9.mol

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1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE Property

Boiling point:: 115-118 °C(Press: 0.01 Torr)
Density: 1.069
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 7.61±0.20(Predicted)
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B230810
Product name: 1-Benzylazepan-4-one
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B230810
Product name: 1-Benzylazepan-4-one
Packaging: 1g
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151123
Product name: 1-Benzyl-hexahydro-4H-azepin-4-one
Packaging: 500mg
Price: $125
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151123
Product name: 1-Benzyl-hexahydro-4H-azepin-4-one
Packaging: 1g
Price: $216
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151123
Product name: 1-Benzyl-hexahydro-4H-azepin-4-one
Packaging: 250mg
Price: $70
Updated: 2021/12/16

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1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE Chemical Properties,Usage,Production

Synthesis

50492-22-3

100-39-0

1208-75-9

Potassium carbonate (K2CO3, 12 g, 88 mmol, 3.0 eq.) was added to acetone (10 mL) as 4-azepinone hydrochloride (1-18, 4.4 g, 29 mmol) and benzyl bromide (5.0 g, 29 mmol, 1.0 eq.). The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the crude reaction mixture was concentrated by evaporation, the residue was dissolved in ethyl acetate and the organic layer was washed with water. The crude product was purified by silica gel column chromatography to afford 1-benzylhexahydroazepin-4-one (1-19, 5.6 g, 95% yield). Mass spectrometric (ESI) analysis showed m/z 204.1 (M + H+).

References

[1] Patent: WO2010/144571, 2010, A1. Location in patent: Page/Page column 133-134
[2] Patent: WO2015/140559, 2015, A1. Location in patent: Page/Page column 50; 51
[3] Patent: US2013/143870, 2013, A1. Location in patent: Paragraph 0489; 0490
[4] Patent: US2013/150341, 2013, A1. Location in patent: Paragraph 0418; 0419
[5] Patent: WO2013/83741, 2013, A1. Location in patent: Page/Page column 98

1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE Suppliers

China 91 Germany 1 India 2 United Kingdom 2 United States 9 Global 105

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shanghai cooperpharm co.,LTD .

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View Lastest Price from 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE manufacturers

Career Henan Chemical Co

Product: 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE 1208-75-9
Price: US $1.00/g
Min. Order: 100g
Purity: 98%min
Supply Ability: G/KG/T
Release date: 2019-12-20

1208-75-9, 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONERelated Search:

6,10-dimethylundecan-2-one 1-METHYLAZEPAN-4-ONE ETHYL 1-BENZYL-5-OXOAZEPANE-4-CARBOXYLATE 1-BENZYL-4-OXOAZEPANE HCL Azepan-4-one N-Benzoyl-4-perhydroazepinone 1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE

1-BENZYL-HEXAHYDRO-4H-AZEPIN-4-ONE

1-Benzylazepan-4-one

1-Benzylhexahydro-4-azepinone

4H-Azepin-4-one,hexahydro-1-(phenylmethyl)-

N-Benzylazepane-4-one

4H-Azepin-4-one

hexahydro-1-(phenylMethyl)-

1-benzyl-4-azepanone

1208-75-9

1208-79-5

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