4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER

Product Name: 4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER
CAS No.: 80051-07-6
Chemical Name: 4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER
Synonyms: Methyl 4-(1-aMinoethyl)benzoate;4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER;Benzoic acid, 4-(1-aminoethyl)-, methyl ester
CBNumber: CB52459685
Molecular Formula: C10H13NO2
Formula Weight: 179.22
MOL File: 80051-07-6.mol

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4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER Property

Boiling point:: 281.5±15.0 °C(Predicted)
Density: 1.089±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 8?+-.0.10(Predicted)
Appearance: Colorless to off-white Solid-liquid mixture

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M328533
Product name: Methyl4-(1-aminoethyl)benzoate
Packaging: 250mg
Price: $165
Updated: 2021/12/16

ChemScene

Product number: CS-M0171
Product name: methyl4-(1-aminoethyl)benzoate
Purity: ≥97.0%
Packaging: 250mg
Price: $75
Updated: 2021/12/16

ChemScene

Product number: CS-M0171
Product name: methyl4-(1-aminoethyl)benzoate
Purity: ≥97.0%
Packaging: 100mg
Price: $102
Updated: 2021/12/16

AK Scientific

Product number: 3829AH
Product name: Methyl4-(1-aminoethyl)benzoate
Packaging: 250mg
Price: $162
Updated: 2021/12/16

ChemScene

Product number: CS-M0171
Product name: methyl4-(1-aminoethyl)benzoate
Purity: ≥97.0%
Packaging: 1g
Price: $188
Updated: 2021/12/16

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4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

3609-53-8

593-51-1

74-89-5

80051-07-6

GENERAL STEPS: Methyl 4-acetylbenzoate (1.07 g, 6 mmol), methylamine (33% ethanol solution, 4.5 mL), methylamine hydrochloride (1.62 g, 24.0 mmol), and sodium cyanoborohydride (0.56 g, 9.0 mmol) were dissolved in a solvent mixture of tetrahydrofuran (12 mL) and methanol (7 mL). The reaction mixture was stirred at 65 °C for 16 hours. Upon completion of the reaction, the reaction solution was concentrated in vacuum and the residue was redissolved in dichloromethane (20 mL) and washed with deionized water (20 mL). The organic phase was dried over anhydrous sodium sulfate and concentrated in vacuum to give the crude methyl 4-(1-aminoethyl)benzoate, which could be used in the next reaction without further purification. Yield: 0.86 g, 75% yield. LCMS analysis (Method B): retention time 0.98 min, purity 89%; m/z 194.05 ([M+H]+, 100%).

References

[1] Patent: WO2010/20556, 2010, A1. Location in patent: Page/Page column 169-170

4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER Suppliers

China 31 India 1 United States 2 Global 34

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80051-07-6, 4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTERRelated Search:

METHYL 4-[AMINO(CYCLOPROPYL)METHYL]BENZOATE METHYL 4,4'-BIPHENYL-R-ALANATE

4-(1-AMINO-ETHYL)-BENZOIC ACID METHYL ESTER

Methyl 4-(1-aMinoethyl)benzoate

Benzoic acid, 4-(1-aminoethyl)-, methyl ester

80051-07-6