(10-Phenyl-9-anthracenyl)boronic acid pinacol ester

ChemicalBook > CAS DataBase List > (10-Phenyl-9-anthracenyl)boronic acid pinacol ester

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester

Product Name: (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
CAS No.: 460347-59-5
Chemical Name: (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
Synonyms: 10-Phenylanthracene-9-boronic Acid Pinacol Ester;(10-Phenyl-9-anthracenyl)boronic acid pinacol ester;9-Phenyl-10-anthracen(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl);9-Phenyl-10-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)anthracene;4,4,5,5-Tetramethyl-2-(10-phenyl-9-anthracenyl)-1,3,2-dioxaborolane;4,4,5,5-Tetramethyl-2-(10-Phenylanthracen-9-Yl)-1,3,2-Dioxaborolane;4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane;9-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-10-phenylanthracene;1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(10-phenyl-9-anthracenyl)-
CBNumber: CB52462210
Molecular Formula: C26H25BO2
Formula Weight: 380.29
MOL File: 460347-59-5.mol

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(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Property

Melting point:: 165.0 to 169.0 °C
Boiling point:: 524.1±19.0 °C(Predicted)
Density: 1.15
form: powder to crystal
color: White to Light yellow

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Safety

HS Code: 2931.90.6000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: T3665
Product name: 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane
Purity: >98.0%(GC)
Packaging: 1g
Price: $43
Updated: 2024/03/01

TCI Chemical

Product number: T3665
Product name: 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane
Purity: >98.0%(GC)
Packaging: 5g
Price: $173
Updated: 2024/03/01

TRC

Product number: T889730
Product name: 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Chem-Impex

Product number: 40044
Product name: 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,98%(GC)
Purity: 98%(GC)
Packaging: 1G
Price: $236.32
Updated: 2021/12/16

Chem-Impex

Product number: 40044
Product name: 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,≥98%(GC)
Purity: ≥98%(GC)
Packaging: 5G
Price: $830.5
Updated: 2021/12/16

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(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Chemical Properties,Usage,Production

Preparation

9-Bromo-10-phenylanthracene (5.8g, 17.4mmol), bis(pinacolato)diboron(6.63 g, 26.1 mmol), Pd(dppf)Cl2 (710 mg, 0.87 mmol), and KOAc (10.23 g, 104.4 mmol) were mixed in a 250mL flask containing 1,4-dioxane (60 mL). The reaction mixture was refluxed for 24h under nitrogen. After it was cooled to room temperature, a dilute hydrochloric acid solution quenched. The mixture was extracted with CH2Cl2 and dried over anhydrous MgSO4. The crude product was concentrated by rotary evaporation and further purified by silica gel column chromatography (CH2Cl2 / petroleum ether (1:1,v/v)) to afford a light yellow powder (4.0 g, 60.4 %). 1H NMR (500 MHz, CDCl3) δ 8.46 (d, J = 8.7 Hz, 2H), 7.65 (d, J = 8.8 Hz, 2H), 7.57 (dq, J = 14.2, 7.0 Hz, 3H), 7.51 – 7.46 (m, 2H), 7.41 (d, J = 7.0 Hz, 2H), 7.34 (dd, J = 8.1, 7.1 Hz, 2H), 1.63 (s, 12H). EI-MS (m/z): Calculated for C26H25BO2: 380.29. Found [M+]: 379.92.

Synthesis of 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (10-Phenyl-9-anthracenyl)boronic acid pinacol ester manufacturers

Shanghai Daken Advanced Materials Co.,Ltd

Product: 4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane 460347-59-5
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 150KG /month
Release date: 2021-11-16

Career Henan Chemical Co

Product: (10-Phenyl-9-anthracenyl)boronic acid pinacol ester 460347-59-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons/month
Release date: 2020-01-09

460347-59-5, (10-Phenyl-9-anthracenyl)boronic acid pinacol esterRelated Search:

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester

4,4,5,5-Tetramethyl-2-(10-phenyl-9-anthracenyl)-1,3,2-dioxaborolane

9-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-10-phenylanthracene

4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane

4,4,5,5-Tetramethyl-2-(10-Phenylanthracen-9-Yl)-1,3,2-Dioxaborolane

1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(10-phenyl-9-anthracenyl)-

10-Phenylanthracene-9-boronic Acid Pinacol Ester

9-Phenyl-10-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)anthracene

9-Phenyl-10-anthracen(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)

460347-59-5

C26H25BO2