ChemicalBook > CAS DataBase List > 1-(5-Bromo-2-fluorophenyl)ethanol
1-(5-Bromo-2-fluorophenyl)ethanol
- Product Name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- CAS No.
- 552331-15-4
- Chemical Name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- Synonyms
- 1-(5-broMo-2-fluorophenyl)ethan-1-ol;1-(5-Bromo-2-fluorophenyl);1-(5-BroMo-2-fluorophenyl)ethano;1-(5-Bromo-2-fluorophenyl)ethanol;5-Bromo-2-fluoro-a-methylbenzenemethanol;Benzenemethanol, 5-bromo-2-fluoro-α-methyl-;5-Bromo-2-fluoro-alpha-methylbenzenemethanol
- CBNumber
- CB52470022
- Molecular Formula
- C8H8BrFO
- Formula Weight
- 219.05
- MOL File
- 552331-15-4.mol
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1-(5-Bromo-2-fluorophenyl)ethanol Property
- Boiling point:
- 254.0±25.0 °C(Predicted)
- Density
- 1.554±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.87±0.20(Predicted)
- Appearance
- Light brown to brown Liquid
- InChI
- InChI=1S/C8H8BrFO/c1-5(11)7-4-6(9)2-3-8(7)10/h2-5,11H,1H3
- InChIKey
- QWIJUQVYIYCHMK-UHFFFAOYSA-N
- SMILES
- CC(C1=CC(Br)=CC=C1F)O
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
AK Scientific
- Product number
- W6927
- Product name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
Oakwood
- Product number
- 211056
- Product name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- Purity
- 95+%
- Packaging
- 5g
- Price
- $150
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0037189
- Product name
- 1-(5-BROMO-2-FLUOROPHENYL)ETHANOL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $156.45
- Updated
- 2021/12/16
AK Scientific
- Product number
- W6927
- Product name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- Packaging
- 5g
- Price
- $203
- Updated
- 2021/12/16
AK Scientific
- Product number
- W6927
- Product name
- 1-(5-Bromo-2-fluorophenyl)ethanol
- Packaging
- 10g
- Price
- $279
- Updated
- 2021/12/16
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1-(5-Bromo-2-fluorophenyl)ethanol Chemical Properties,Usage,Production
Synthesis
75-16-1
93777-26-5
552331-15-4
1. 1.4 M methylmagnesium bromide (THF/toluene solution) (36.9 mL) was added slowly and dropwise to a solution of 5-bromo-2-fluorobenzaldehyde (10.0 g, 49.26 mmol) in anhydrous ethyl ether (60 mL) at 0 °C. 2. The reaction mixture was stirred at 0 °C for 30 min. 3. Upon completion of the reaction, the reaction was quenched sequentially with water (50 mL) and 1 N HCl (10 mL). The reaction was quenched with water (50 mL) and 1N HCl (10 mL). 4. The organic phase was separated and dried over anhydrous magnesium sulfate. 5. The desiccant was removed by filtration and the filtrate was concentrated under reduced pressure to afford 1-(5-bromo-2-fluorophenyl)ethanol (10.8 g, 100% yield). 6. The product was confirmed by mass spectrometry (ESI) at m/z 218 [M + 1]+, 220 [M + 2]+ .
References
[1] Patent: US2008/242694, 2008, A1. Location in patent: Page/Page column 41
[2] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 20, p. 6832 - 6846
[3] Patent: WO2009/11880, 2009, A2. Location in patent: Page/Page column 95
[4] Patent: WO2006/44860, 2006, A2. Location in patent: Page/Page column 23
[5] Patent: US2006/142307, 2006, A1. Location in patent: Page/Page column 24
1-(5-Bromo-2-fluorophenyl)ethanol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-(5-Bromo-2-fluorophenyl)ethanol manufacturers
Career Henan Chemical Co
- Product
- 1-(5-Bromo-2-fluorophenyl)ethanol 552331-15-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-02