methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride
- Product Name
- methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride
- CAS No.
- 90942-47-5
- Chemical Name
- methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride
- Synonyms
- Methyl 5-(aminomethyl);-2-chlorobenzoate hydrochloride;methyl 5-(aminomethyl)-2-chlorobenzoate.HCl;methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride;5-AMinoMethyl-2-chloro-benzoic acid Methyl ester hydrochloride
- CBNumber
- CB52490088
- Molecular Formula
- C9H11Cl2NO2
- Formula Weight
- 236.09514
- MOL File
- 90942-47-5.mol
methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride Property
- Melting point:
- 217-220 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C9H10ClNO2.ClH/c1-13-9(12)7-4-6(5-11)2-3-8(7)10;/h2-4H,5,11H2,1H3;1H
- InChIKey
- RVCZOTOWWCOGCQ-UHFFFAOYSA-N
- SMILES
- C(OC)(=O)C1=CC(CN)=CC=C1Cl.[H]Cl
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M286683
- Product name
- methyl5-(aminomethyl)-2-chlorobenzoatehydrochloride
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- HCH0369483
- Product name
- METHYL-5-(AMINOMETHYL)-2-CHLOROBENZOATE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.58
- Updated
- 2021/12/16
- Product number
- 5165AC
- Product name
- Methyl5-(aminomethyl)-2-chlorobenzoatehydrochloride
- Packaging
- 5g
- Price
- $717
- Updated
- 2021/12/16
- Product number
- CM157581
- Product name
- methyl5-(aminomethyl)-2-chlorobenzoatehydrochloride
- Purity
- 95+%
- Packaging
- 1g
- Price
- $143
- Updated
- 2021/12/16
- Product number
- CM157581
- Product name
- methyl5-(aminomethyl)-2-chlorobenzoatehydrochloride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $393
- Updated
- 2021/12/16
methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride Chemical Properties,Usage,Production
Synthesis
1427158-17-5
90942-47-5
Methyl 5-((tert-butoxycarbonylamino)methyl)-2-chlorobenzoate (100 mg, 0.334 mmol) was used as a raw material, which was dissolved in 1 mL of EtOAc solution saturated with HCl and the reaction was stirred for 2 hours at room temperature. Upon completion of the reaction, the reaction mixture was concentrated and ground with pentane to yield 80 mg of the final target product, methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride. The structure of the product was confirmed by 1H NMR (300 MHz, DMSO-d6): δ 8.20 (br s, 3H), 7.95 (s, 1H), 7.67 (s, 2H), 4.00 (s, 2H), 3.88 (s, 3H).
References
[1] Patent: WO2013/38308, 2013, A1. Location in patent: Page/Page column 40; 41
[2] Patent: WO2013/72825, 2013, A1. Location in patent: Page/Page column 38
[3] Patent: US2013/210844, 2013, A1. Location in patent: Paragraph 0298; 0299
[4] Patent: WO2014/167444, 2014, A1. Location in patent: Page/Page column 34; 35
methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride Preparation Products And Raw materials
Raw materials
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