ChemicalBook > CAS DataBase List > XtalFluor-E

XtalFluor-E

Product Name
XtalFluor-E
CAS No.
63517-29-3
Chemical Name
XtalFluor-E
Synonyms
DiethylaMinodifluorosulfiniuM tetrafluoroborate;1-fluoro-2,4,6-trimethylpyridin-1-ium;(Diethylamino)difluorosulfonium tetrafluoroborate;triethylphosphanium;tetrafluoroboranuide;3,5-dichloro-1-fluoropyridin-1-ium;Xtalfiuor-E;XtalFluor-E;XtalFluor-E(R);1-butylpyridin-1-ium
CBNumber
CB52491469
Molecular Formula
C4H10BF6NS
Formula Weight
228.9953192
MOL File
63517-29-3.mol
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XtalFluor-E Property

Melting point:
84-87℃
storage temp. 
-20°C
InChIKey
YLNKFQWRRIXZPJ-UHFFFAOYSA-N
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Safety

Hazard Codes 
T
Risk Statements 
23/24/25-34
Safety Statements 
26-36/37/39-45
RIDADR 
UN 2923 8/PG 3
WGK Germany 
3
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
719439
Product name
XtalFluor-E®
Packaging
5G
Price
$52.8
Updated
2024/03/01
Sigma-Aldrich
Product number
719439
Product name
XtalFluor-E®
Packaging
25G
Price
$204
Updated
2024/03/01
Sigma-Aldrich
Product number
719439
Product name
XtalFluor-E®
Packaging
250G
Price
$1600
Updated
2024/03/01
Sigma-Aldrich
Product number
719439
Product name
XtalFluor-E®
Packaging
1KG
Price
$5190
Updated
2024/03/01
TRC
Product number
X746320
Product name
XtalFluor-E
Packaging
10g
Price
$220
Updated
2021/12/16
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XtalFluor-E Chemical Properties,Usage,Production

Description

XtalFluor-E, [Et2NSF2]BF4, is best known as a useful, versatile and inexpensive commercially available reagent for the deoxyfluorination of carbonyl compounds and alcohols. Although XtalFluor-E is commonly used in combination with an exogenous fluoride source as a deoxofluorinating reagent, it has also been widely employed in other chemical transformations such as dehydration, cyclodehydration, ring expansion, formylation, and proto-functionalization, etc.

Uses

XtalFluor-E can be used as convenient crystalline highly chemoselective deoxofluorination reagent with a broad substrate scopeDeoxofluorination reagent with a better safety profile.

Application

Convenient crystalline highly chemoselective deoxofluorination reagent with a broad substrate scope
Deoxofluorination reagent with a better safety profile, that doesn′t generate corrosive HF which makes it suitable for use in standard borosilicate vessels, and does not react violently with water
Reactant for:
Preparation of fluorodisaccharides
Triisopropylsilanethiol was recently reported by MacMillian and coworkers to be used as an organocatalyst, in tandem with Ir(III) specifically Aldrich product 688096, in photoredox catalysis. This approach directly couples a cyano-containing arene with an allylic sp3 C-H bond.

References

XtalFluor-E: A useful and versatile reagent in organic transformations
(DOI): 10.1016/j.jfluchem.2019.06.006
XtalFluorE effects the C3H sulfenylation of indoles to form di indole sulfides
(DOI): 10.1002/ejoc.202101394

XtalFluor-E Preparation Products And Raw materials

Raw materials

Preparation Products

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XtalFluor-E Suppliers

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View Lastest Price from XtalFluor-E manufacturers

Zjartschem
Product
XtalFluor-E 63517-29-3
Price
US $0.00/kg
Min. Order
100g
Purity
97%
Supply Ability
500g,1kg,5kg,10kg,50kg,100kg...
Release date
2019-02-13
WUHAN FORTUNA CHEMICAL CO., LTD
Product
(Diethylamino)difluorosulfonium Tetrafluoroborate 63517-29-3
Price
US $0.00/KG
Min. Order
1KG
Purity
95%min
Supply Ability
30tons/month
Release date
2023-02-22
Henan Aochuang Chemical Co.,Ltd.
Product
XtalFluor-E 63517-29-3
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1Ton
Release date
2022-10-09

63517-29-3, XtalFluor-ERelated Search:

XtalFluor-M

  • N,N-Diethyl-S,S-difluorosulfiliminium tetrafluoroborate
  • XtalFluor-E(R)
  • DiethylaMinodifluorosulfiniuM tetrafluoroborate
  • diethylamino(difluoro)sulfanium,tetrafluoroborate
  • XtalFluor-E
  • Xtalfiuor-E
  • (Diethylamino)difluorosulfonium tetrafluoroborate
  • DAST difluorosulfinium salt
  • N-(Difluoro-λ4-sulfanylidene)-N-ethyl-ethanaminium tetrafluoroborate
  • N,N-Diethylamino-S,S-difluorosulfinium tetrafluoroborate
  • (difluoro-λ-sulfanylidene)diethylazanium
  • tetrafluoroboranuide
  • 4-acetyl-3-phenylpiperazin-1-ium
  • iethylamino(difluoro)sulfanium,tetrafluoroborate
  • 1-butylpyridin-1-ium
  • di-tert-butyl(phenyl)phosphanium
  • 4-(difluoro--sulfanylidene)-4-morpholin-4-ylium
  • 2-(methoxycarbonyl)thiophene-3-diazonium
  • 4-tert-butyl-2,6-dimethyl-1-pyran-1-ylium
  • 2-bromo-1-methylpyridin-1-ium
  • methyldiphenylsulfanium
  • 1-propyl-2-(1,2,2,2-tetrafluoroethyl)pyridin-1-ium
  • 1-methoxy-4-phenylpyridin-1-ium
  • 1-fluoro-2,4,6-trimethylpyridin-1-ium
  • 2-ethyl-1,3-dimethyl-1H-1,3-benzodiazol-3-ium
  • 1-(dimethyl-2H-1,3-dithiol-2-ylidene)-1-piperidin-1-ylium
  • 1-(cyanomethyl)-2,4,6-trimethylpyridin-1-ium
  • 1,3-dimethyl-2-(trifluoromethyl)-1H-1,3-benzodiazol-3-ium
  • 1,3-bis(propan-2-yl)-4,5-dihydro-1H-imidazol-3-ium
  • phenyl[2-(trimethylsilyl)ethynyl]iodanium
  • N,N-dimethylcyclopentaniminium
  • triethylphosphanium
  • trimethyldisulfanium
  • 2,4,6-trimethyl-1-phenyl-1-pyridin-1-ylium
  • 2,4,6-trimethyl-1-(prop-2-en-1-yl)pyridin-1-ium
  • 3-(4-bromophenyl)-4-[1,3]thiazolo[3,2-a]pyridin-4-ylium
  • 1-benzyl-2,4,6-trimethylpyridin-1-ium
  • 1-benzyl-2,6-diethyl-4-phenylpyridin-1-ium
  • 1-[chloro(pyrrolidin-1-yl)methylidene]-1-pyrrolidin-1-ylium
  • 1-[(4-methoxyphenyl)methyl]pyridin-1-ium
  • ethynyl(phenyl)iodanium
  • ethyldiphenylsulfanium
  • [(dimethylamino)[(2-oxo-1,2-dihydropyridin-1-yl)oxy]methylidene]dimethylazanium
  • (dimethylamino)(methyl)oxo(phenyl)--sulfanylium
  • 3,5-dichloro-1-fluoropyridin-1-ium
  • 3,5-bis(trifluoromethyl)benzene-1-diazonium
  • (4-chlorophenyl)(pentafluoroethyl)iodanium
  • 2-tert-butyl-1,3-dimethyl-1H-1,3-benzodiazol-3-ium
  • diethylamino(difluoro)sulfanium
  • TIANFU-CHEM XtalFluor-E
  • (difluoro-λ?-sulfanylidene)-diethyl-ammonium
  • DAST difluorosulfinium saltXtalFluor-E
  • Ethanaminium, N-(difluoro-λ4-sulfanylidene)-N-ethyl-, tetrafluoroborate(1-) (1:1)
  • (difluoro-lambda4-sulfanylidene)-diethyl-ammonium tetrafluoroborate
  • 63517-29-3
  • C4H10F2NSBF4
  • Chemical Synthesis
  • Fluorination