ChemicalBook > CAS DataBase List > 1H-Imidazole-1-sulfonyl azide hydrochloride

1H-Imidazole-1-sulfonyl azide hydrochloride

Product Name
1H-Imidazole-1-sulfonyl azide hydrochloride
CAS No.
952234-36-5
Chemical Name
1H-Imidazole-1-sulfonyl azide hydrochloride
Synonyms
1H-Imidazole-1-sulfonyl azide hydrochloride;Imidazole-1-sulfonyl azide HCl;Imidazole-1-sulfonyl azide, HCl salt;Imidazole-1-sulfonyl azide hydrochloride;1H-Imidazole-1-sulphonylazidehydrochloride;N-diazoimidazole-1-sulfonamide hydrochloride;1H-Imidazole-1-sulfonyl Azide Hydrochloride Salt
CBNumber
CB52547096
Molecular Formula
C3H3N5O2S.HCl
Formula Weight
210
MOL File
952234-36-5.mol
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1H-Imidazole-1-sulfonyl azide hydrochloride Property

Melting point:
102-104℃
storage temp. 
2-8°C
solubility 
Methanol (Slightly), Water (Slightly)
form 
Solid
color 
White to Off-White
Stability:
Hygroscopic, forms hydrazoic acid on prolonged storage and on contact with water
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Safety

HS Code 
2933299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H242Heating may cause a fire

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P234Keep only in original container.

P235Keep cool.

P240Ground/bond container and receiving equipment.

P370+P378In case of fire: Use … for extinction.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

TRC
Product number
I385635
Product name
1H-Imidazole-1-sulfonylAzideHydrochlorideSalt
Packaging
100mg
Price
$60
Updated
2021/12/16
Apolloscientific
Product number
OR301255
Product name
1H-Imidazole-1-sulphonylazidehydrochloride
Packaging
1g
Price
$308
Updated
2021/12/16
SynQuest Laboratories
Product number
8H69-5-07
Product name
1H-Imidazole-1-sulfonyl azide hydrochloride
Packaging
1g
Price
$340
Updated
2021/12/16
SynQuest Laboratories
Product number
8H69-5-07
Product name
1H-Imidazole-1-sulfonyl azide hydrochloride
Packaging
5G
Price
$592
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0292789
Product name
IMIDAZOLE-1-SULFONYL AZIDE HYDROCHLORIDE
Purity
95.00%
Packaging
1G
Price
$652.58
Updated
2021/12/16
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1H-Imidazole-1-sulfonyl azide hydrochloride Chemical Properties,Usage,Production

Uses

1H-Imidazole-1-sulfonyl azide hydrochloride is an azide salt, which can be used as an intermediate in organic synthesis and material chemistry, and is commonly used as a diazotropic transfer reagent in the field of chemical synthesis. It is also used in the synthesis of bioactive molecules and organic functional materials.

Synthesis

1H-Imidazole-1-sulfonyl azide hydrochloride was synthesised by a series of chemical reactions using 1H-imidazole as raw material, and the specific reflective steps are as follows:
Sulfurylchloride (16.2 mL, 0.2 mol) was added dropwise to an ice-cooled suspension ofNaN3 (13.0 g, 0.2 mol) in anhydrous acetonitrile (200 mL) and themixture was stirred overnight. Imidazole (27.2 g, 0.4 mol) was addedportionwise to the ice-cooled mixture and the slurry was stirred for 5 h. Themixture was diluted by EA (400 mL) and 400 mL of water was added. The organiclayer was washed by water (2x400 mL), followed by saturated NaHCO3solution (2x400 mL) and brine (400 mL). The organic layer was dried over Na2SO4.Asolution of HCl/EtOH, obtained by dropwise addition of AcCl (21.3 mL, 0.3 mol)to ice-cooled dry ethanol (75 mL) was added dropwise to the filtrate withstirring, which was dried to get the white solid (36 g, 96% yield), which waskept desiccator under N2 atmosphere.LC-MS(ESI): [M+1]+ = 173.80, tR = 2.73 min.1H NMR (400 MHz, D2O) δ 9.43 (s, 1H), 8.00 (s, 1H), 7.60 (s, 1H).13C NMR (101 MHz, D2O) δ 137.66, 123.01, 120.20.

1H-Imidazole-1-sulfonyl azide hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1H-Imidazole-1-sulfonyl azide hydrochloride manufacturers

Career Henan Chemical Co
Product
Imidazole-1-sulfonyl azide hydrochloride 952234-36-5
Price
US $1.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
200KG
Release date
2018-12-23

952234-36-5, 1H-Imidazole-1-sulfonyl azide hydrochlorideRelated Search:


  • 1H-Imidazole-1-sulfonyl azide hydrochloride
  • Imidazole-1-sulfonyl azide hydrochloride
  • 1H-Imidazole-1-sulphonylazidehydrochloride
  • Imidazole-1-sulfonyl azide HCl
  • 1H-Imidazole-1-sulfonyl Azide Hydrochloride Salt
  • Imidazole-1-sulfonyl azide, HCl salt
  • N-diazoimidazole-1-sulfonamide hydrochloride
  • 952234-36-5
  • 952234-36-6
  • C3H3N5O2SClH
  • C3H3N5O2SHCl