3-broMo-6,9-diphenyl-9H-carbazole
- Product Name
- 3-broMo-6,9-diphenyl-9H-carbazole
- CAS No.
- 1160294-85-8
- Chemical Name
- 3-broMo-6,9-diphenyl-9H-carbazole
- Synonyms
- DPCBA-B;3-Bromo-6,9-diphenylcarbazole;3-Bromo-6,9-diphenylcarbazole>3-broMo-6,9-diphenyl-9H-carbazole;9H-Carbazole, 3-bromo-6,9-diphenyl-;3-broMo-6,9-diphenyl-9H-carbazole ISO 9001:2015 REACH
- CBNumber
- CB52553400
- Molecular Formula
- C24H16BrN
- Formula Weight
- 398.29
- MOL File
- 1160294-85-8.mol
3-broMo-6,9-diphenyl-9H-carbazole Property
- Melting point:
- 143.0 to 147.0 °C
- Boiling point:
- 564.2±32.0 °C(Predicted)
- Density
- 1.32±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Almost white
Safety
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- B4795
- Product name
- 3-Bromo-6,9-diphenylcarbazole
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $36
- Updated
- 2025/07/31
- Product number
- B4795
- Product name
- 3-Bromo-6,9-diphenylcarbazole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $128
- Updated
- 2025/07/31
- Product number
- B997235
- Product name
- 3-Bromo-6,9-diphenyl-9H-carbazole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 30935
- Product name
- 3-Bromo-6,9-diphenylcarbazole,≥98%(GC)
- Purity
- ≥98%(GC)
- Packaging
- 1G
- Price
- $50.17
- Updated
- 2021/12/16
- Product number
- 2639AA
- Product name
- 3-Bromo-6,9-diphenyl-9H-carbazole
- Packaging
- 5g
- Price
- $137
- Updated
- 2021/12/16
3-broMo-6,9-diphenyl-9H-carbazole Chemical Properties,Usage,Production
Chemical Properties
white powder
Synthesis
1028648-09-0
1160294-85-8
Step 1: Synthesis of 3-bromo-6,9-diphenyl-9H-carbazole In a 300 mL Erlenmeyer flask, 4.8 g (15 mmol) of 3,9-diphenyl-9H-carbazole and 250 mL of mixed solvent (ethyl acetate: toluene = 4:1) were added. The mixture was stirred for 30 min to ensure complete dissolution. Subsequently, 2.7 g (15 mmol) of N-bromosuccinimide (NBS) was slowly added and the reaction mixture was continuously stirred for 48 hours. After completion of the reaction, the reaction mixture was washed sequentially with saturated sodium bicarbonate solution and saturated brine. The organic layer was separated and dried with anhydrous magnesium sulfate. After drying, the magnesium sulfate was removed by filtration and the filtrate was concentrated to obtain an oil. A small amount of ethanol was added to the oil and the solid was induced to precipitate by ultrasonic treatment. The precipitated solid was collected by diafiltration to give 5.4 g of white powdery product in 90% yield.
References
[1] Patent: WO2009/72587, 2009, A1. Location in patent: Page/Page column 243-244
[2] Patent: TW2017/2233, 2017, A. Location in patent: Paragraph 0197; 0200; 0201
[3] Patent: WO2012/121561, 2012, A1. Location in patent: Page/Page column 26-27
3-broMo-6,9-diphenyl-9H-carbazole Preparation Products And Raw materials
Raw materials
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View Lastest Price from 3-broMo-6,9-diphenyl-9H-carbazole manufacturers
- Product
- 3-Bromo-6,9-diphenyl-9H-carbazole 1160294-85-8
- Price
- US $0.00/kg
- Min. Order
- 20kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2024-10-15
- Product
- 3-bromo-6,9-diphenyl-9H-carbazole 1160294-85-8
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-17
- Product
- 3-Bromo-6,9-diphenyl-9H-carbazole 1160294-85-8
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-02