1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE

Product Name: 1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE
CAS No.: 216076-11-8
Chemical Name: 1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE
Synonyms: 1-(2-chlorophenyl)-2-(4-pyridyl)ethanone;1-(2-chlorophenyl)-2-(4-pyridinyl)Ethanone;1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE;Ethanone, 1-(2-chlorophenyl)-2-(4-pyridinyl)-
CBNumber: CB5257148
Molecular Formula: C13H10ClNO
Formula Weight: 231.68
MOL File: 216076-11-8.mol

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1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE Property

storage temp.: Inert atmosphere,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 9402AH
Product name: 1-(2-Chloro-phenyl)-2-pyridin-4-yl-ethanone
Packaging: 250mg
Price: $401
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0314147
Product name: 1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE
Purity: 98.00%
Packaging: 5MG
Price: $496.46
Updated: 2021/12/16

Ambeed

Product number: A117585
Product name: 1-(2-Chlorophenyl)-2-(pyridin-4-yl)ethanone
Purity: 95+%
Packaging: 100mg
Price: $40
Updated: 2021/12/16

Ambeed

Product number: A117585
Product name: 1-(2-Chlorophenyl)-2-(pyridin-4-yl)ethanone
Purity: 95+%
Packaging: 250mg
Price: $78
Updated: 2021/12/16

Ambeed

Product number: A117585
Product name: 1-(2-Chlorophenyl)-2-(pyridin-4-yl)ethanone
Purity: 95+%
Packaging: 1g
Price: $205
Updated: 2021/12/16

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1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE Chemical Properties,Usage,Production

Synthesis

108-89-4

289686-74-4

216076-11-8

1. A solution of 4-methylpyridine (1.07 g, 11.5 mmol) in THF (10.0 mL) was added slowly and dropwise to a solution of tetrahydrofuran (THF, 20.0 mL) containing lithium diisopropylammonium (6.5 mL, 1.6 M in cyclohexane, 10.4 mmol) at -78°C. 2. The dry ice bath was removed and the reaction mixture was stirred at 0 °C for 30 min and then re-cooled to -78 °C. 3. A solution of 2-chloro-N-methoxy-N-methylbenzamide (2.39 g, 12 mmol) in THF (10.0 mL) was added dropwise to the reaction mixture. 4. The reaction mixture was gradually warmed to room temperature and stirred overnight. 5. The resulting white solid was collected by filtration and dissolved in ethyl acetate. 6. The organic phase was washed sequentially with water and brine and then dried with anhydrous magnesium sulfate. 7. Vacuum concentration of the dried organic phase afforded the target product 1-(2-chlorophenyl)-2-(pyridin-4-yl)ethanone (1.09 g, 4.7 mmol, 47% yield) as a white solid.

References

[1] Patent: WO2009/91759, 2009, A1. Location in patent: Page/Page column 49
[2] Patent: WO2009/91760, 2009, A1. Location in patent: Page/Page column 41

1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE Suppliers

China 16 India 1 United States 4 Global 21

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216076-11-8, 1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONERelated Search:

1-(2,4-DICHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE 1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE 1-PHENYL-2-PYRIDIN-4-YL-ETHANONE

1-(2-CHLORO-PHENYL)-2-PYRIDIN-4-YL-ETHANONE

1-(2-chlorophenyl)-2-(4-pyridinyl)Ethanone

Ethanone, 1-(2-chlorophenyl)-2-(4-pyridinyl)-

1-(2-chlorophenyl)-2-(4-pyridyl)ethanone

216076-11-8