ChemicalBook > CAS DataBase List > 6-BroMopyridine-2-sulfonaMide

6-BroMopyridine-2-sulfonaMide

Product Name
6-BroMopyridine-2-sulfonaMide
CAS No.
856013-04-2
Chemical Name
6-BroMopyridine-2-sulfonaMide
Synonyms
6-BroMopyridine-2-sulfonaMide;2-Pyridinesulfonamide, 6-bromo-
CBNumber
CB52628672
Molecular Formula
C5H5BrN2O2S
Formula Weight
237.07
MOL File
856013-04-2.mol
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6-BroMopyridine-2-sulfonaMide Property

storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB141691
Product name
6-Bromopyridine-2-sulfonamide
Packaging
50mg
Price
$51
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141691
Product name
6-Bromopyridine-2-sulfonamide
Packaging
100mg
Price
$89
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141691
Product name
6-Bromopyridine-2-sulfonamide
Packaging
250mg
Price
$177.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141691
Product name
6-Bromopyridine-2-sulfonamide
Packaging
500mg
Price
$310
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0367861
Product name
6-BROMOPYRIDINE-2-SULFONAMIDE
Purity
95.00%
Packaging
5MG
Price
$500.27
Updated
2021/12/16
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6-BroMopyridine-2-sulfonaMide Chemical Properties,Usage,Production

Synthesis

1135871-89-4

856013-04-2

b) 6-Bromo-N-(tert-butyl)pyridine-2-sulfonamide (478 mg, 1.63 mmol) was dissolved in trifluoroacetic acid (TFA, 2 mL), and the reaction mixture was stirred for 3 hours at 60 °C. After completion of the reaction, TFA was evaporated under reduced pressure and the residue was treated with a solvent mixture of petroleum ether and ethyl ether (Et2O) to precipitate a brown solid. The solid was collected by filtration and ground three times with ether to give the final white solid product 6-bromopyridine-2-sulfonamide (125 mg, 32% yield). The product was characterized by 1H NMR (DMSO-d6, ppm): 7.98 (t, J=7.5 Hz, 1H), 7.91 (dd, J=7.5 and 1.2 Hz, 1H), 7.87 (dd, J=7.5 and 0.9 Hz, 1H).

References

[1] Patent: WO2009/39553, 2009, A1. Location in patent: Page/Page column 87

6-BroMopyridine-2-sulfonaMide Preparation Products And Raw materials

Raw materials

Preparation Products

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856013-04-2, 6-BroMopyridine-2-sulfonaMideRelated Search:


  • 6-BroMopyridine-2-sulfonaMide
  • 2-Pyridinesulfonamide, 6-bromo-
  • 856013-04-2