1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene

Product Name: 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene
CAS No.: 170098-88-1
Chemical Name: 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene
Synonyms: 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene;Benzene, 1-chloro-4-fluoro-2-methyl-5-nitro-
CBNumber: CB52645415
Molecular Formula: C7H5ClFNO2
Formula Weight: 189.57
MOL File: 170098-88-1.mol

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1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene Property

storage temp.: 2-8°C
Appearance: Light brown to yellow Solid-Liquid Mixture

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Safety

HS Code: 2904990090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C585020
Product name: 1-Chloro-4-fluoro-2-methyl-5-nitrobenzene
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C585020
Product name: 1-Chloro-4-fluoro-2-methyl-5-nitrobenzene
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: PC900714
Product name: 1-Chloro-4-fluoro-2-methyl-5-nitrobenzene
Purity: 97%
Packaging: 1g
Price: $90
Updated: 2021/12/16

Apolloscientific

Product number: PC900714
Product name: 1-Chloro-4-fluoro-2-methyl-5-nitrobenzene
Purity: 97%
Packaging: 5g
Price: $190
Updated: 2021/12/16

AK Scientific

Product number: 8715AA
Product name: 1-Chloro-4-fluoro-2-methyl-5-nitrobenzene
Packaging: 5g
Price: $249
Updated: 2021/12/16

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1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene Chemical Properties,Usage,Production

Synthesis

33406-96-1

170098-88-1

The general procedure for the synthesis of 2-chloro-5-fluoro-4-nitrotoluene from 2-chloro-5-fluorotoluene was as follows: to a stirred concentrated solution of 2-chloro-5-fluorotoluene (0.500 g, 3.46 mmol, Lancaster, for direct use) was added H2SO4 (5.0 mL) slowly at 0 °C. Subsequently, KNO3 (0.350 g, 3.46 mmol) was added all at once. The reaction mixture was gradually warmed to 28 °C and stirred at this temperature overnight. Upon completion of the reaction, the mixture was quenched by pouring it into ice (50 g) and extracted with ether (2 x 50 mL). The combined ether layers were dried with anhydrous Na2SO4 and subsequently concentrated under reduced pressure to remove the solvent. The obtained oily product was further dried under vacuum to give 0.616 g (94% yield) of 2-chloro-5-fluoro-4-nitrotoluene as an oil, which was used directly in the subsequent reaction.1H NMR (CDCl3) data were as follows: δ 2.459 (s, 3H), 7.193 (d, 1H, J=11.1 Hz), 8.083 (d, 1H, J= 6.6Hz).

References

[1] Patent: WO2007/107566, 2007, A1. Location in patent: Page/Page column 45
[2] Patent: WO2007/36718, 2007, A2. Location in patent: Page/Page column 53
[3] Patent: WO2008/119721, 2008, A1. Location in patent: Page/Page column 60
[4] Journal of Organic Chemistry, 1995, vol. 60, # 18, p. 5838 - 5842
[5] Patent: US5631373, 1997, A

1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene Suppliers

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View Lastest Price from 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene manufacturers

Career Henan Chemical Co

Product: 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene 170098-88-1
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-02-13

170098-88-1, 1-Chloro-4-fluoro-2-Methyl-5-nitrobenzeneRelated Search:

1-Chloro-4-fluoro-2-Methyl-5-nitrobenzene

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170098-88-1