4-BroMo-5-nitrobenzene-1,2-diaMine
- Product Name
- 4-BroMo-5-nitrobenzene-1,2-diaMine
- CAS No.
- 113269-07-1
- Chemical Name
- 4-BroMo-5-nitrobenzene-1,2-diaMine
- Synonyms
- 4-BroMo-5-nitrobenzene-1,2-diaMine;1,2-Benzenediamine, 4-bromo-5-nitro-
- CBNumber
- CB52651612
- Molecular Formula
- C6H6BrN3O2
- Formula Weight
- 232.03
- MOL File
- 113269-07-1.mol
4-BroMo-5-nitrobenzene-1,2-diaMine Property
- Boiling point:
- 394.1±37.0 °C(Predicted)
- Density
- 1.901±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 1.46±0.10(Predicted)
N-Bromosuccinimide Price
- Product number
- 7825DU
- Product name
- 4-Bromo-5-nitrobenzene-1,2-diamine
- Packaging
- 100mg
- Price
- $347
- Updated
- 2021/12/16
- Product number
- A199434
- Product name
- 4-Bromo-5-nitrobenzene-1,2-diamine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $657
- Updated
- 2021/12/16
- Product number
- 113269071
- Product name
- 4-Bromo-5-nitrobenzene-1,2-diamine
- Packaging
- 1g
- Price
- $808
- Updated
- 2021/12/16
- Product number
- A199434
- Product name
- 4-Bromo-5-nitrobenzene-1,2-diamine
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $132
- Updated
- 2021/12/16
- Product number
- 113269071
- Product name
- 4-Bromo-5-nitrobenzene-1,2-diamine
- Packaging
- 100mg
- Price
- $231
- Updated
- 2021/12/16
4-BroMo-5-nitrobenzene-1,2-diaMine Chemical Properties,Usage,Production
Synthesis
113269-05-9
113269-07-1
General procedure for the synthesis of 4-bromo-5-nitrobenzene-1,2-diamine from N,N'-(4-bromo-5-nitro-1,2-phenylene)bis(4-methylbenzenesulfonamide): N,N'-(4-bromo-5-nitro-1,2-phenylene)bis(4-methylbenzenesulfonamide) (0.92 g. 1.71 mmol) was placed in a 10 mL round bottom flask. 90% sulfuric acid (2 mL) was added slowly and the reaction mixture was placed in an oil bath at 85°C with stirring and reflux for 2 hours. Upon completion of the reaction, the mixture was removed and cooled to room temperature and subsequently poured into 50 mL of water. The pH was adjusted to 9 with ammonia, at which point a red solid precipitated. After the mixture was cooled, filtration was carried out and the solid was washed twice with cold water. 4-Bromo-5-nitrobenzene-1,2-diamine (0.34 g, 86.8% yield) was finally obtained.
References
[1] Heterocycles, 1987, vol. 26, # 9, p. 2433 - 2442
[2] Patent: CN108341791, 2018, A. Location in patent: Paragraph 0013; 0014; 0017
4-BroMo-5-nitrobenzene-1,2-diaMine Preparation Products And Raw materials
Raw materials
Preparation Products
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