4-(bis(4-iodophenyl)aMino)benzaldehyde

Product Name: 4-(bis(4-iodophenyl)aMino)benzaldehyde
CAS No.: 808758-81-8
Chemical Name: 4-(bis(4-iodophenyl)aMino)benzaldehyde
Synonyms: 4-(bis(4-iodophenyl)aMino)benzaldehyde;Benzaldehyde, 4-[bis(4-iodophenyl)amino]-;4-[Bis(4-iodophenyl)amino]benzaldehyde >4-(4-iodo-N-(4-iodophenyl)anilino)benzaldehyde;4-(bis(4-iodophenyl)aMino)benzaldehyde USP/EP/BP;4-(bis(4-iodophenyl)aMino)benzaldehydephenyl)amino)benzaldehyde,Benzaldehyde, 4-[bis[4-[3,6-bis(1,1-dimethylethyl)-9H-carba
CBNumber: CB52708125
Molecular Formula: C19H13I2NO
Formula Weight: 525.12
MOL File: 808758-81-8.mol

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4-(bis(4-iodophenyl)aMino)benzaldehyde Property

Melting point:: 139.0 to 143.0 °C
Boiling point:: 560.6±45.0 °C(Predicted)
Density: 1.899±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: powder to crystal
pka: -6.96±0.50(Predicted)
color: Light yellow to Yellow to Orange
InChI: InChI=1S/C19H13I2NO/c20-15-3-9-18(10-4-15)22(19-11-5-16(21)6-12-19)17-7-1-14(13-23)2-8-17/h1-13H
InChIKey: HIUBJHKIRVFTOM-UHFFFAOYSA-N
SMILES: C(=O)C1=CC=C(N(C2=CC=C(I)C=C2)C2=CC=C(I)C=C2)C=C1

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Safety

HS Code: 2922.39.5000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B4543
Product name: 4-[Bis(4-iodophenyl)amino]benzaldehyde
Purity: >95.0%(GC)
Packaging: 200mg
Price: $247
Updated: 2024/03/01

Matrix Scientific

Product number: 127023
Product name: 4-(Bis(4-iodophenyl)amino)benzaldehyde
Purity: >95%
Packaging: 1g
Price: $396
Updated: 2021/12/16

AK Scientific

Product number: 6235AL
Product name: 4-(Bis(4-iodophenyl)amino)benzaldehyde
Packaging: 1g
Price: $584
Updated: 2021/12/16

Abosyn

Product number: 61-11185
Product name: 4-(Bis(4-iodophenyl)amino)benzaldehyde
Purity: 95-98%
Packaging: 5g
Price: $695
Updated: 2021/12/16

Chemenu

Product number: CM278928
Product name: 4-(Bis(4-iodophenyl)amino)benzaldehyde
Purity: 95+%
Packaging: 10g
Price: $701
Updated: 2021/12/16

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4-(bis(4-iodophenyl)aMino)benzaldehyde Chemical Properties,Usage,Production

Synthesis

4181-05-9

808758-81-8

4-(Bis(4-iodophenyl)amino)benzaldehyde (3) was synthesized as follows: in a 100 mL two-necked flask equipped with a nitrogen inlet, a magnetic stirrer and a condenser, 4-(diphenylamino)benzaldehyde (2) (3.8 g, 13.9 mmol), potassium iodide (3.0 g, 18.1 mmol), acetic acid (45.0 mL), and deionized water (5.0 mL ). The reaction mixture was heated to 80 °C and potassium iodate (2.98 g, 13.9 mmol) was added quickly. The resulting mixture was stirred continuously at 80 °C for 5 hours. Upon completion of the reaction, the solution was cooled to room temperature and slowly poured into ice water with stirring. The resulting yellow precipitate was collected by filtration and washed with 5% mass fraction NaHSO3 solution (40.0 mL). After filtration, the target product 4-(bis(4-iodophenyl)amino)benzaldehyde (3) was obtained as a yellow solid (7.0 g, 13.4 mmol, 96% yield). The 1H NMR spectrum of the product was in agreement with literature reports (Ning et al., 2007).

References

[1] Journal of Polymer Science, Part A: Polymer Chemistry, 2010, vol. 48, # 15, p. 3417 - 3430
[2] Chemical Papers, 2015, vol. 70, # 2, p. 218 - 230
[3] Tetrahedron Letters, 2007, vol. 48, # 33, p. 5877 - 5881
[4] Tetrahedron, 2008, vol. 64, # 24, p. 5736 - 5742
[5] New Journal of Chemistry, 2009, vol. 33, # 10, p. 2120 - 2127

4-(bis(4-iodophenyl)aMino)benzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(bis(4-iodophenyl)aMino)benzaldehyde Suppliers

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808758-81-8

809758-81-8

C19H13I2NO