ChemicalBook > CAS DataBase List > Methyl 4-aMino-2-Methyl-5-nitrobenzoate
Methyl 4-aMino-2-Methyl-5-nitrobenzoate
- Product Name
- Methyl 4-aMino-2-Methyl-5-nitrobenzoate
- CAS No.
- 1260848-51-8
- Chemical Name
- Methyl 4-aMino-2-Methyl-5-nitrobenzoate
- Synonyms
- Methyl 4-aMino-2-Methyl-5-nitrobenzoate;Benzoic acid, 4-amino-2-methyl-5-nitro-, methyl ester
- CBNumber
- CB52710162
- Molecular Formula
- C9H10N2O4
- Formula Weight
- 210.19
- MOL File
- 1260848-51-8.mol
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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Property
- Boiling point:
- 403.7±40.0 °C(Predicted)
- Density
- 1.332±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- -2.34±0.25(Predicted)
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N-Bromosuccinimide Price
TRC
- Product number
- M563125
- Product name
- Methyl4-amino-2-methyl-5-nitrobenzoate
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 119066
- Product name
- Methyl 4-amino-2-methyl-5-nitrobenzoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $630
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 119066
- Product name
- Methyl 4-amino-2-methyl-5-nitrobenzoate
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $252
- Updated
- 2021/12/16
Abosyn
- Product number
- 61-2883
- Product name
- Methyl4-amino-2-methyl-5-nitrobenzoate
- Purity
- 95%-98%
- Packaging
- 0.25g
- Price
- $315
- Updated
- 2021/12/16
Ambeed
- Product number
- A186000
- Product name
- Methyl4-amino-2-methyl-5-nitrobenzoate
- Purity
- 95%
- Packaging
- 100mg
- Price
- $55
- Updated
- 2021/12/16
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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Chemical Properties,Usage,Production
Synthesis
1163287-01-1
1260848-51-8
Step 3. Ammonia (g) was passed into a solution of THF (180 mL) containing methyl 4-fluoro-2-methyl-5-nitrobenzoate (30 g, 140.74 mmol) and the reaction was carried out for 5 hours at room temperature. Upon completion of the reaction, the reaction was quenched with water (500 mL). The solid was collected by filtration to afford methyl 4-amino-2-methyl-5-nitrobenzoate as a yellow solid (24.5 g, 83% yield).LC/MS (ES, m/z): [M+H]+ 211.0.1H-NMR (300 MHz, CDCl3): δ8.85(s, 1H), 6.64(s, 1H), 3.88(s, 3H) , 2.61(s, 3H).
References
[1] Patent: US2012/277224, 2012, A1. Location in patent: Page/Page column 61
Methyl 4-aMino-2-Methyl-5-nitrobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Suppliers
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