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Methyl 4-aMino-2-Methyl-5-nitrobenzoate

Product Name
Methyl 4-aMino-2-Methyl-5-nitrobenzoate
CAS No.
1260848-51-8
Chemical Name
Methyl 4-aMino-2-Methyl-5-nitrobenzoate
Synonyms
Methyl 4-aMino-2-Methyl-5-nitrobenzoate;Benzoic acid, 4-amino-2-methyl-5-nitro-, methyl ester
CBNumber
CB52710162
Molecular Formula
C9H10N2O4
Formula Weight
210.19
MOL File
1260848-51-8.mol
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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Property

Boiling point:
403.7±40.0 °C(Predicted)
Density 
1.332±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
-2.34±0.25(Predicted)
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
M563125
Product name
Methyl4-amino-2-methyl-5-nitrobenzoate
Packaging
50mg
Price
$90
Updated
2021/12/16
Matrix Scientific
Product number
119066
Product name
Methyl 4-amino-2-methyl-5-nitrobenzoate
Purity
95+%
Packaging
1g
Price
$630
Updated
2021/12/16
Matrix Scientific
Product number
119066
Product name
Methyl 4-amino-2-methyl-5-nitrobenzoate
Purity
95+%
Packaging
250mg
Price
$252
Updated
2021/12/16
Abosyn
Product number
61-2883
Product name
Methyl4-amino-2-methyl-5-nitrobenzoate
Purity
95%-98%
Packaging
0.25g
Price
$315
Updated
2021/12/16
Ambeed
Product number
A186000
Product name
Methyl4-amino-2-methyl-5-nitrobenzoate
Purity
95%
Packaging
100mg
Price
$55
Updated
2021/12/16
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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Chemical Properties,Usage,Production

Synthesis

1163287-01-1

1260848-51-8

Step 3. Ammonia (g) was passed into a solution of THF (180 mL) containing methyl 4-fluoro-2-methyl-5-nitrobenzoate (30 g, 140.74 mmol) and the reaction was carried out for 5 hours at room temperature. Upon completion of the reaction, the reaction was quenched with water (500 mL). The solid was collected by filtration to afford methyl 4-amino-2-methyl-5-nitrobenzoate as a yellow solid (24.5 g, 83% yield).LC/MS (ES, m/z): [M+H]+ 211.0.1H-NMR (300 MHz, CDCl3): δ8.85(s, 1H), 6.64(s, 1H), 3.88(s, 3H) , 2.61(s, 3H).

References

[1] Patent: US2012/277224, 2012, A1. Location in patent: Page/Page column 61

Methyl 4-aMino-2-Methyl-5-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 4-aMino-2-Methyl-5-nitrobenzoate Suppliers

Hunan Hui Bai Shi Biotechnology Co., Ltd.
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China
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1260848-51-8, Methyl 4-aMino-2-Methyl-5-nitrobenzoateRelated Search:


  • Methyl 4-aMino-2-Methyl-5-nitrobenzoate
  • Benzoic acid, 4-amino-2-methyl-5-nitro-, methyl ester
  • 1260848-51-8