2-Fluoro-N-Methyl-5-nitroaniline

Product Name: 2-Fluoro-N-Methyl-5-nitroaniline
CAS No.: 110729-51-6
Chemical Name: 2-Fluoro-N-Methyl-5-nitroaniline
Synonyms: 2-Fluoro-N-Methyl-5-nitroaniline;Benzenamine, 2-fluoro-N-methyl-5-nitro-
CBNumber: CB52710955
Molecular Formula: C7H7FN2O2
Formula Weight: 170.14
MOL File: 110729-51-6.mol

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2-Fluoro-N-Methyl-5-nitroaniline Property

Boiling point:: 270.3±30.0 °C(Predicted)
Density: 1.361±0.06 g/cm3(Predicted)
pka: 2.12±0.25(Predicted)
InChI: InChI=1S/C7H7FN2O2/c1-9-7-4-5(10(11)12)2-3-6(7)8/h2-4,9H,1H3
InChIKey: YWKHWTYJUYVMND-UHFFFAOYSA-N
SMILES: C1(NC)=CC([N+]([O-])=O)=CC=C1F

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Safety

HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: F593230
Product name: 2-Fluoro-n-methyl-5-nitroaniline
Packaging: 1g
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: PC904455
Product name: 2-Fluoro-N-methyl-5-nitroaniline
Purity: 95%
Packaging: 10g
Price: $841
Updated: 2021/12/16

AK Scientific

Product number: 0387CV
Product name: 2-Fluoro-N-methyl-5-nitroaniline
Packaging: 25g
Price: $1022
Updated: 2021/12/16

Apolloscientific

Product number: PC904455
Product name: 2-Fluoro-N-methyl-5-nitroaniline
Purity: 95%
Packaging: 1g
Price: $189
Updated: 2021/12/16

AK Scientific

Product number: 0387CV
Product name: 2-Fluoro-N-methyl-5-nitroaniline
Packaging: 5g
Price: $357
Updated: 2021/12/16

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2-Fluoro-N-Methyl-5-nitroaniline Chemical Properties,Usage,Production

Uses

2-Fluoro-N-Methyl-5-nitroaniline can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical and pharmaceutical production process.

Synthesis

2-fluoro-5-nitroaniline (20.0g, 128.2mmol) and paraformaldehyde (16.0g, 533.3mmol) was dissolved in 500mL of methanol then stirred at room temperature. Then added dropwise NaOMe (3.4g, 63mmol) in methanol 100mL. The reaction was stirred at room temperature for 16 hours then was added NaBH4 (9.7g, 255.2mmol) in two aliquots, stirred for 15 minutes. LCMS traced the reaction. After completion of the reaction was poured into 1M KOH aqueous solution, and stirred to precipitate a solid. Filtered to give a yellow solid 2-fluoro-N-methyl-5-nitroaniline (19.0g, 87% yield).

2-Fluoro-N-Methyl-5-nitroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Fluoro-N-Methyl-5-nitroaniline Suppliers

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110729-51-6, 2-Fluoro-N-Methyl-5-nitroanilineRelated Search:

2-Fluoro-N-Methyl-5-nitroaniline

Benzenamine, 2-fluoro-N-methyl-5-nitro-

110729-51-6