3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

Product Name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
CAS No.: 1233200-57-1
Chemical Name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Synonyms: 3-Bromo-5'-phenyl-1,1';3-Bromo-5'-phenyl-m-terphenyl;5'-(3-Bromophenyl)-m-terphenyl;3',5'-Diphenyl-3-broMobiphenyl;1-(3-BROMOPHENYL)-3,5-DIPHENYLBENZENE;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl;5'-(3-Bromophenyl)-1,1':3',1''-terphenyl;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl>
CBNumber: CB52717404
Molecular Formula: C24H17Br
Formula Weight: 385.3
MOL File: 1233200-57-1.mol

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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Property

Melting point:: 112.0 to 116.0 °C
Boiling point:: 497.8±14.0 °C(Predicted)
Density: 1.278±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
color: White to Light yellow

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Safety

HS Code: 2903.99.8001

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B4888
Product name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity: >98.0%(GC)
Packaging: 1g
Price: $37
Updated: 2025/07/31

TCI Chemical

Product number: B4888
Product name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity: >98.0%(GC)
Packaging: 5g
Price: $182
Updated: 2025/07/31

TRC

Product number: B997463
Product name: 3-Bromo-5''-phenyl-1,1'':3'',1''''-terphenyl
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 6003AL
Product name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Packaging: 100g
Price: $1200
Updated: 2021/12/16

Arctom

Product number: AS021651
Product name: 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity: 97%
Packaging: 5g
Price: $112
Updated: 2021/12/16

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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Chemical Properties,Usage,Production

Synthesis

591-18-4

1036378-83-2

1233200-57-1

GENERAL STEPS: Compound I-8 (50 g, 140 mmol) and 2-([1,1':3',1''-terphenyl]-5'-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (43.7 g, 154 mmol) were dissolved in 0.45 L of tetrahydrofuran (THF), and tetrakis(triphenylphosphine)palladium was added under nitrogen protection ( 1.62 g, 1.40 mmol). Subsequently, saturated aqueous potassium carbonate solution (48.4 g, 350 mmol) was added and the reaction mixture was heated to reflux at 80 °C for 12 hours. After completion of the reaction, the reaction solution was poured into water and the organic phase was extracted with dichloromethane (DCM). The organic phase was dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The resulting residue was purified by fast column chromatography to afford the target product 3-bromo-5'-phenyl-1,1':3',1''-terphenyl (Compound I-15, 41.5 g, 77% yield).

References

[1] Patent: KR2015/117173, 2015, A. Location in patent: Paragraph 0239-0241
[2] Patent: KR2016/19747, 2016, A. Location in patent: Paragraph 0234-0237

3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Suppliers

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