ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE
- Product Name
- ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE
- CAS No.
- 148550-51-0
- Chemical Name
- ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE
- Synonyms
- Ethyl 2-(Methylsulfonyl)-5-pyrimidinecarboxylate;ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE;ETHYL 2-(METHYLSULPHONYL)PYRIMIDINE-5-CARBOXYLATE;Ethyl 2-(methylsulfonyl)pyrimidine-5-carboxylate 95%;2-(Methylsulfonyl)-5-pyrimidinecarboxylic acid ethyl ester;5-Pyrimidinecarboxylic acid, 2-(methylsulfonyl)-, ethyl ester;ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE ISO 9001:2015 REACH
- CBNumber
- CB5286362
- Molecular Formula
- C8H10N2O4S
- Formula Weight
- 230.24
- MOL File
- 148550-51-0.mol
ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE Property
- Boiling point:
- 407.7±37.0 °C(Predicted)
- Density
- 1.338±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- -4.99±0.22(Predicted)
- Appearance
- Off-white to yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- OR55185
- Product name
- Ethyl2-(methylsulfonyl)pyrimidine-5-carboxylate
- Purity
- 95%
- Packaging
- 100mg
- Price
- $218
- Updated
- 2021/12/16
- Product number
- OR55185
- Product name
- Ethyl2-(methylsulfonyl)pyrimidine-5-carboxylate
- Purity
- 95%
- Packaging
- 250mg
- Price
- $327
- Updated
- 2021/12/16
- Product number
- CHM0376240
- Product name
- ETHYL-2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.09
- Updated
- 2021/12/16
- Product number
- OR55185
- Product name
- Ethyl2-(methylsulfonyl)pyrimidine-5-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $754
- Updated
- 2021/12/16
- Product number
- CD11251854
- Product name
- Ethyl2-(methylsulfonyl)pyrimidine-5-carboxylate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $850
- Updated
- 2021/12/16
ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE Chemical Properties,Usage,Production
Synthesis
73781-88-1
148550-51-0
Step 2: Synthesis of ethyl 2-(methylsulfonyl)pyrimidine-5-carboxylate (121); Sulfide 120 (0.424 g, 2.14 mmol) was dissolved in dichloromethane (DCM, 9 mL), and a DCM (9 mL) solution of 3-chloroperoxybenzoic acid (mCPBA, 2.0 g) was slowly added. The reaction mixture was stirred at room temperature for 100 min. Upon completion of the reaction, the reaction was quenched with aqueous Na2S2O3, diluted with DCM and washed with saturated NaHCO3 solution. The organic phase was dried over anhydrous MgSO4, filtered and concentrated to give the target product 121 (0.374 g, 76% yield). [0726] MS: m/z 230.1 (calculated), 230.9 (measured).
References
[1] Synthetic Communications, 1993, vol. 23, # 6, p. 715 - 723
[2] Patent: WO2007/118137, 2007, A1. Location in patent: Page/Page column 105
[3] Chemical Biology and Drug Design, 2016, vol. 87, # 3, p. 472 - 477
[4] Patent: CN106279044, 2017, A. Location in patent: Paragraph 0026; 0030; 0070; 0071
[5] Patent: WO2012/117421, 2012, A1. Location in patent: Page/Page column 44
ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from ETHYL 2-(METHYLSULFONYL)PYRIMIDINE-5-CARBOXYLATE manufacturers
- Product
- ethyl 2-(methylsulfonyl)pyrimidine-5-carboxylate 148550-51-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.0% min
- Supply Ability
- 100 tons min
- Release date
- 2021-05-12